Synthesis and characterization of hydroxyapatite powder from natural Camelus bone

Jaber, Hassanen; Hammood, Ali Sabea; Parvin, Nader

doi:10.1007/s41779-017-0120-0

Cited by 66 publications

(40 citation statements)

References 21 publications

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“…Therefore, various chemical routes have been introduced for HAp synthesis including hydrothermal, sol-gel, mechano-chemical, precipitation, and polymer-assisted methods. HAp can also be fabricated from bio-waste or natural resources including clam shell [24], bovine [25], camel bones [26], corals [27], cuttlefish [28], and fish bone [17,29].…”

Section: Abstract a R T I C L E I N F O R M A T I O Nmentioning

confidence: 99%

Hydroxyapatite Consolidated by Zirconia: Applications for Dental Implant

Sharifianjazi

Pakseresht

Asl

et al. 2020

jcc

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Section: Abstract a R T I C L E I N F O R M A T I O Nmentioning

confidence: 99%

Hydroxyapatite Consolidated by Zirconia: Applications for Dental Implant

Sharifianjazi

Pakseresht

Asl

et al. 2020

jcc

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“…3. A phosphate group is located at the 960 cm −1 , 430 cm −1 , 1030, and 1045 cm −1 [11], and the amide which is located at 1076 cm −1 is present at raw powder which is removed after calcination process. The spectrum of the powder before calcination illustrates that, at 1114 cm −1 a weak intensity is not observed in the spectrum of the powders, and after calcination process, this is associated to the existence the organic materials (C-H) before calcination process.…”

Section: Raman Spectroscopymentioning

confidence: 99%

“…Kim et al [10] studied the short-and long-range-order structural analysis of in situ created biphasic calcium phosphates, and the results show that Ca/P molar ratio, lattice parameters, and the crystal phases of in situ formed BCP consist of β-TCP and HAp that were controlled by the degree of calcium deficiency of calcium phosphate precursors. Jaber et al [11] utilized the camelus bone to synthesize HAp powders, and the results present that powders obtained at calcining temperature (1000 °C) were a pure hydroxyapatite with the Ca/P ratio of 1.6557. Hammood et al [12] used the bovine femur bone to synthesize natural hydroxyapatite, and the results show the optimal calcination temperature to obtain near to pure hydroxyapatite at 900 °C.…”

Section: Introductionmentioning

confidence: 99%

Effect of calcination temperature on characterization of natural hydroxyapatite prepared from carp fish bones

et al. 2019

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Hydroxyapatite is one of the most common bio-ceramic materials which is currently used in the biomedical field. The development of hydroxyapatite is due to their crystallographic and chemical similarity to the hard tissue of human body. The present study aims to prepare hydroxyapatite from a bio-waste material (carp fish bone) as an ecofriendly and inexpensive source by calcination treatment. The calcination process was applied at various calcining temperatures; the heating rate was kept constant at 10 °C min −1. FTIR results proved the formation of hydroxyapatite at 950 °C due to the founding peaks corresponding to phosphate (632 cm −1) and hydroxyl (3572 cm −1). XRD analysis confirmed the formation of HAp at 950 °C by the presence three main peaks: (211), (112), and (300), which correspond to the characteristic peaks of hydroxyapatite. Raman analyses which displayed the calcining process remove organic components from a bones matrix. AFM showed that the size of particles is ranged between nano and microns. EDS analysis found that the Ca/P reaches 1.6589 for fish bone after calcination at 950 °C, which is close to stoichiometric HAp (1.67).

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“…Nosoudi et al found the hydroxyapatite containing 35 μg etidronate showed low early strength, but high strength after soaking in simulated body fluid (SBF) [14]. Jaber et al, utilized the camelus bone to synthesize HAp powders, and the results showed that powders obtained at calcination temperature (1000 °C) was a pure HAp with the Ca/P ratio of 1.6557 [15]. The aim at this work is to approach the optimal temperature to obtain hydroxyapatite nanoparticles from the bovine femur bone.…”

Section: Introductionmentioning

confidence: 99%

Access to Optimal Calcination Temperature for Nanoparticle Synthesis from Hydroxyapatite Bovine Femur Bone Waste

Hammood¹,

Hassan²,

Alkhafagy³

2017

Nano BioMed ENG

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Hydroxyapatite (HAp) is one of the vital and bioactive materials that are commonly used in biomedical field and concentrated in clinical area. It is a bio-ceramic powder synthesized by using different bio-waste materials such as bovine femur bone. In this study, the bovine femur bone powder was prepared to obtain nano powder. The purpose of this study was to reach the optimal temperature to obtain nanoparticles HAp. The resulted powder was calcinated in a furnace at different temperatures (900, 950, 1000, 1050 and 1100 °C) for 2 h at the heating rate of 10 °C/min and cooled slowly in a furnace. Results showed, the formation of pure HAp by the presence of peaks corresponding to (PO 4 ) 3-at 632/cm and OH -at 3,572/cm in fourier transformation infrared spectroscopy (FTIR). For the calcined samples, there were three main peaks of 211, 112 and 300 planes at 2θ near 31.8, 32.2 and 32.9 respectively. The amorphous raw bones were transformed into crystalline phase and the lattice parameters for HAp c and a were calculated in X-ray diffraction (XRD), Raman analysis showed that the calcination process removed the organic compound from the bovine femur bones matrix. Scanning electron microscopy (SEM) and energy dispersive X-ray analysis (EDX) showed that the shape of the granules was irregular, containing quantities of oxygen, magnesium, sodium and carbon; the ratio of calcium to phosphate was calculated, Atomic force microscopy (AFM) showed that the particles sizes ranged from nanometers to microns. EDX result found that the calcium to phosphate ratio reached 1.7058 after calcination at 950 °C which was close to stoichiometric hydroxyapatite (1.67). This result implied the formation of pure HAp phase at 950 °C.

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Synthesis and characterization of hydroxyapatite powder from natural Camelus bone

Cited by 66 publications

References 21 publications

Hydroxyapatite Consolidated by Zirconia: Applications for Dental Implant

Hydroxyapatite Consolidated by Zirconia: Applications for Dental Implant

Effect of calcination temperature on characterization of natural hydroxyapatite prepared from carp fish bones

Access to Optimal Calcination Temperature for Nanoparticle Synthesis from Hydroxyapatite Bovine Femur Bone Waste

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