Synthesis and characterization of Fe (III) complex of an azo dye derived from (2-amino-5-chlorophenyl) phenyl methanone

Mini, S.; Meena, Sher Singh; Bhatt, Pramod; Sadasivan, V.; Vidya, V.G.

doi:10.1063/1.4810575

Cited by 4 publications

(3 citation statements)

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“…33,34 Here axial ligands attached to central atom are not liberated on to the area of electrode during CV measurements and the reduction process has a reversible character. 35,36,37,38,39,40 The second harmonic generation performance of BNAP and its complexes had been determined. The performance of the sample was set side by side with microcrystalline powder of (potassium dihydrogen phosphate) KDP.…”

Section: H (Gauss) → Fig 5 Esr Spectrum Of [Cu(bnap)2(h2o)2]mentioning

confidence: 99%

Synthesis, spectroscopic characterization and biological activities of some metal complexes with new heterocyclic azodye ligand 2-(2-hydroxynaphthalen-1-yl azo)-pyridin-3-ol

Vidya¹,

Sadasivan²

2023

10.5267/j.ccl

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Metal complexes of [2-(2-hydroxynaphthalen-1-ylazo)-pyridin-3-ol] are derived from 2-amino-3-hydroxypyridine and β-naphthol was synthesized and characterized by thermal, spectral and analytical tools. The ligand was reacted with Mn(II), Fe(II), Co(II), Ni(II), Cu(II) and Zn(II) in 1:2 stoichiometry. The IR spectra confirms the azo ligand coordination to metal ions via azo nitrogen and phenolic oxygen of pyridine after deprotonation. Both IR and 1HNMR spectra recorded involvement of deprotonated hydroxyl groups with proton displacement. The magnified fluorescence was shown by Mn(II) and Ni(II) complexes. None of the prepared ligands or complexes show any NLO activity with KDP as standard. The DNA cleavage and anticancerous activities done. The influence of zinc chelates on cure characteristics of rubber compounds was estimated based on rheometer measurements. The ligand and metal complexes are tested in vitro against some bacteria and fungi species. The antioxidant activities, DNA cleavage and anticancerous activities done. Ligand and its complexes catalysed cleavage of DNA.

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Section: H (Gauss) → Fig 5 Esr Spectrum Of [Cu(bnap)2(h2o)2]mentioning

confidence: 99%

Synthesis, spectroscopic characterization and biological activities of some metal complexes with new heterocyclic azodye ligand 2-(2-hydroxynaphthalen-1-yl azo)-pyridin-3-ol

Vidya¹,

Sadasivan²

2023

10.5267/j.ccl

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“…The Mössbauer effect provides a powerful probe to chemical state and the environment of Fe(III) ion [16]. The Mössbauer spectra of the Fe(III) complex of FABP was recorded at room temperature.…”

Section: Mössbauer Spectramentioning

confidence: 99%

Synthesis and spectral studies of metal complexes of a Schiff base derived from (2-amino-5-chlorophenyl)phenyl methanone

Mini

Sadasivan

Meena

et al. 2015

Spectrochimica Acta Part A: Molecular and Biomolecular Spectros

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“…The ligand RABP is prepared by diazotizing 2-amino-5-chlorobenzophenone and coupling with resorcinol (Mini S., et al, 2013). The resulting product was recrystallised from DMF.…”

Section: Synthesis Of [2-chloro-5-(24-dihydroxy Phenylazo)phenyl]phementioning

confidence: 99%

SYNTHESIS AND CHARACTERIZATION OF Ni(II) AND Zn(II) COMPLEXES OF AN AZODYE DERIVED FROM 2-AMINO-5-CHLORO BENZOPHENONE.

Ijar¹

2016

IJAR

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2-amino-5-cholorobenzophenone, 1,3 benzenediol , NMR Ni(II) and Zn(II) complexes were synthesized using the azodye derived from 2-amino-5-chloro benzophenone and 1,3-benzene diol. The complexes were characterized by elemental analysis, metal estimation, electrolytic conducatance, amd magnetic susceptibility measurements. Their characterization were further confirmed by spectral techniques like FTIR, FTNMR, Electronic and Mass spectra Nickel and the zinc complexes were subjected to antimicrobial study. The results indicate the metal and the azodye coordinated in the ratio 1:2. The complexes exhibits non-electrolytic behavior..

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Synthesis and characterization of Fe (III) complex of an azo dye derived from (2-amino-5-chlorophenyl) phenyl methanone

Cited by 4 publications

References 0 publications

Synthesis, spectroscopic characterization and biological activities of some metal complexes with new heterocyclic azodye ligand 2-(2-hydroxynaphthalen-1-yl azo)-pyridin-3-ol

Synthesis, spectroscopic characterization and biological activities of some metal complexes with new heterocyclic azodye ligand 2-(2-hydroxynaphthalen-1-yl azo)-pyridin-3-ol

Synthesis and spectral studies of metal complexes of a Schiff base derived from (2-amino-5-chlorophenyl)phenyl methanone

SYNTHESIS AND CHARACTERIZATION OF Ni(II) AND Zn(II) COMPLEXES OF AN AZODYE DERIVED FROM 2-AMINO-5-CHLORO BENZOPHENONE.

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