Surface Morphology and Crystallographic Orientation of Electrodeposited Fe Film

Abstract

Assistant ProfessorThe crystallographic structure and surface morphology of Fe films electrodeposited in three kinds of baths were studied in detail by SEM and XRD. Fe deposits were prepared in a sulfate bath, chloride bath and sulfamate bath. The surface morphology of Fe deposits on Ni-P amorphous substrate were found to vary according to the electrodeposition bath composition. The (211) plane appeared to be the dominant orientation of deposited films for all baths examined in this study.

Facile synthesis and electromagnetic wave absorption properties of magnetic carbon fiber coated with Fe–Co alloy by electroplating

“…At the beginning of the electroplating process, the atoms nucleate on the sites where the electric current density is higher, since the oxidized surfaces of the CFs are not smooth, small spots appear on the surfaces of the CFs. Then the atoms diffuse around and coatings are gradually formed [12]. During this process, two main factors are determined by electroplating temperature, the so-called ion transport speed in the bath and the atomic diffusion speed in the coating.…”

The Relationship between Microstructure and the Thermal Equilibrium Diagram of Au-Co Alloy Electrodeposit

“…4) did not show diffraction peaks of the Co crystal, and the reason for this is undetermined. In our previous studies, the phase structure of Ag-Co alloy, 12) Au-Ni alloy 13) and Au-Fe alloy 14) plated films, the XRD peaks of the element with a higher melting point displayed broadening, indicating a fine crystalline form near an amorphous state. Therefore, it is considered that the Co crystal of Au-Co alloy films in this study is also composed of fine crystals that are almost amorphous.…”

Structure Control Theory of Plated Film —Part of Surface Morphology—

“…, Cd 11) , Co 12) , Cr 13) , Cu 14) , Fe 15) , Ni 16,17) , Pt 18) , Ru 19) , Sn 20,21) , Zn 22) )，そして 26 種類の二元合金(Ag Co 23,24) , Al Mn 25 27) , Ag Cu 28) , Au Ni 29) , Au Pd 30,31) , Au Sn 32) , Co Cu 33,34) , Co Fe 35) , Co Ni 36) , Co S 37) , Co W 38) , Cu Ni 39) , Cu Pb 40) , Cu Sn 41) , Fe Mo 42) , Co Mo 42) , Ni Mo 42) , Fe Ni 43,44) , Fe W 45) , Fe Zn 46) , In Sn 47) , Ni B 48 50) , Ni P 51 53) , Ni S 54) , Ni Sn 55 58) , Ni W 59 …”