2016
DOI: 10.1080/20548923.2016.1239868
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Studying a Funerary Roman Vessel Glass Collection from Patras, Greece: An Interdisciplinary Characterisation and Use Study

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Cited by 7 publications
(7 citation statements)
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“…The soil samples were dried overnight at 70°C and pellets were made that then were recorded with the aid of a portable X-Rays Fluorescence (p-XRF) set Bruker Tracer III SD aiming at their chemical characterization (Liritzis and Zacharias 2011). The instrumental parameters are described in length at Palamara et al 2016; data quantification was made using S1PXRF software and the-built-in calibration curve for soils and ceramics. In order to optimize the analytical range, two settings were used: (1) an unfiltered low-energy excitation mode (high voltage set at 15 kV) for the analysis of major and minor elements with an atomic number, Z, between 11 and 26; and (2) an Al/Ti filtered high-energy excitation mode (high voltage set at 40 kV) for the analysis of minor and trace elements with an atomic number Z>26.…”
Section: Methodology and Analysismentioning
confidence: 99%
“…The soil samples were dried overnight at 70°C and pellets were made that then were recorded with the aid of a portable X-Rays Fluorescence (p-XRF) set Bruker Tracer III SD aiming at their chemical characterization (Liritzis and Zacharias 2011). The instrumental parameters are described in length at Palamara et al 2016; data quantification was made using S1PXRF software and the-built-in calibration curve for soils and ceramics. In order to optimize the analytical range, two settings were used: (1) an unfiltered low-energy excitation mode (high voltage set at 15 kV) for the analysis of major and minor elements with an atomic number, Z, between 11 and 26; and (2) an Al/Ti filtered high-energy excitation mode (high voltage set at 40 kV) for the analysis of minor and trace elements with an atomic number Z>26.…”
Section: Methodology and Analysismentioning
confidence: 99%
“…A portable Bruker Tracer III SD was used, and data quantification was made using S1PXRF software (Zacharias et al 2018). In order to optimise the analytical range, two settings were used: (1) an unfiltered low-energy excitation mode (high voltage set at 15 kV) for the analysis of major and minor elements with an atomic number, Z, between 11 and 26; and (2) an Al/Ti filtered high-energy excitation mode (high voltage set at 40 kV) for the analysis of minor and trace elements with an atomic number Z>26. The chemical composition was further examined in the Laboratory of Archaeometry at the University of the Peloponnese using Scanning Electron Microscopy coupled with an Energy Dispersive Analyser (SEM/EDS) (Palamara et al 2016). Fresh fractures of the tiles were prepared and analysed further with a JEOL JSM-6510LV device, coupled with an EDS by Oxford Systems.…”
Section: Fig 32mentioning
confidence: 99%
“…The chemical composition was further examined in the Laboratory of Archaeometry at the University of the Peloponnese using Scanning Electron Microscopy coupled with an Energy Dispersive Analyser (SEM/EDS) (Palamara et al 2016). Fresh fractures of the tiles were prepared and analysed further with a JEOL JSM-6510LV device, coupled with an EDS by Oxford Systems.…”
Section: Fig 32mentioning
confidence: 99%
“…The accuracy and precision of this SEM-EDS setting has been described in detail elsewhere (Palamara et al 2016). Generally, all the major oxides in glass represent high precision (error < 5%), with the exception of CaO which presents a deviation from the true value of approximately 10-15%.…”
Section: Sem-eds Analysis In Greecementioning
confidence: 99%
“…The leached areas become enriched in silica and other elements that are not as soluble, for example alumina, manganese and iron oxides. Enrichment of other insoluble components such lead, tin, and antimony can occur (Freestone 2001;Doménech-Carbó et al 2006;Palamara et al 2016). Enrichment of lead and antimony were detected in the Lofkënd opaque white glasses (Muros and Zacharias, 2019, table 3).…”
Section: Composition Of Leached Surfacesmentioning
confidence: 99%