“…The XRD pattern of studied samples corresponded to bismuth sodium titanate and bismuth potassium titanate numbers 36-0153 and 36-0339, respectively. This observed mixed phase well agrees with previous reported [6]. However, the phase of KNbO3 was not detected in the XRD patterns.…”
supporting
confidence: 92%
“…These BNTs have a high opportunity for replacement modified lead based perovskite materials in electronic devices [1][2][3][4]. Among the lead-free ceramics, BNT-BKT ceramic has been focused owing to the existence of the combined phase at morphotropic phase boundary (MPB) located at x = 0.16-0.20 [5,6]. It shows the enhance many properties such as a dielectric, piezoelectric, and electric-field-induced strain properties.…”
This research reports the physical and mechanical properties of (1-x) Bi0.5(Na0.81K0.19)0.5TiO3-xKNbO3 (x=0.00-0.06) ceramics. The Modified Bi0.5(Na0.81K0.19)0.5TiO3 ceramics were synthesized by solid state reaction technique. The mixed oxides powders were calcined at 850 °C, 4 h and sintered at 1120 °C, 2 h to form pure phase perovskite and the optimum bulk density, respectively. The phase formation of the modified ceramic samples was determined by X-ray diffraction technique. All of the modified Bi0.5(Na0.81K0.19)0.5TiO3 ceramics exhibited a single perovskite phase. The bulk densities of the modified ceramic samples were 5.41±0.27-5.75±0.28 g/cm3 using the Archimedes’ method. The microstructure was revealed by the scanning electron microscope. The rectangular-like shape was found of all studied ceramics which had the grain size between 1.31±0.02-1.56±0.03 mm. The mechanical properties were studied by both Vickers and Knoop microhardness tester. The results are discussed in term of the relation among hardness properties, Young’s modulus, and fracture toughness.
“…The XRD pattern of studied samples corresponded to bismuth sodium titanate and bismuth potassium titanate numbers 36-0153 and 36-0339, respectively. This observed mixed phase well agrees with previous reported [6]. However, the phase of KNbO3 was not detected in the XRD patterns.…”
supporting
confidence: 92%
“…These BNTs have a high opportunity for replacement modified lead based perovskite materials in electronic devices [1][2][3][4]. Among the lead-free ceramics, BNT-BKT ceramic has been focused owing to the existence of the combined phase at morphotropic phase boundary (MPB) located at x = 0.16-0.20 [5,6]. It shows the enhance many properties such as a dielectric, piezoelectric, and electric-field-induced strain properties.…”
This research reports the physical and mechanical properties of (1-x) Bi0.5(Na0.81K0.19)0.5TiO3-xKNbO3 (x=0.00-0.06) ceramics. The Modified Bi0.5(Na0.81K0.19)0.5TiO3 ceramics were synthesized by solid state reaction technique. The mixed oxides powders were calcined at 850 °C, 4 h and sintered at 1120 °C, 2 h to form pure phase perovskite and the optimum bulk density, respectively. The phase formation of the modified ceramic samples was determined by X-ray diffraction technique. All of the modified Bi0.5(Na0.81K0.19)0.5TiO3 ceramics exhibited a single perovskite phase. The bulk densities of the modified ceramic samples were 5.41±0.27-5.75±0.28 g/cm3 using the Archimedes’ method. The microstructure was revealed by the scanning electron microscope. The rectangular-like shape was found of all studied ceramics which had the grain size between 1.31±0.02-1.56±0.03 mm. The mechanical properties were studied by both Vickers and Knoop microhardness tester. The results are discussed in term of the relation among hardness properties, Young’s modulus, and fracture toughness.
“…), 3,[17][18][19][20][21] as well as with ABO 3 -type perovskites. [21][22][23][24][25][26][27][28][29][30] These studies suggest that the base composition and the nature of chemical modiers signicantly affect the ferroelectric and piezoelectric properties of BNT-based ceramics. Recently, codoping of impurities into A-and B-sites at the same time was found to be very effective in enhancing the electric-eldinduced strain response.…”
A phase diagram of A- and B-site co-substituted lead-free incipient piezoceramics is schematically constructed on the basis of crystal structure and electromechanical, dielectric and piezoelectric properties.
“…17) Thank to well solidsolution with lead-free Bi 0.5 (Na,K) 0.5 TiO 3 -based ceramics, Ullah et al reported the highest value of S max /E max of 391 pm/V for 5 mol.% BiAlO 3 solid solution in Bi 0.5 (Na 0.8 -K 0.2 ) 0.5 TiO 3 which resulted from transition from the coexistence of rhombohedral and tetragonal phase into pseudocubic phase. 18 21) In fact, co-modification at A-site and B-site further enhanced the S max /E max up to 579 pm/V obtained in lead-free 0.99Bi 0.5 (Na 0.78 K 0.22 ) 0.5 TiO 3 0.01(Bi 0.5 -La 0.5 )AlO 3 composition, resulting from distorted tetragonal structure. 22) These results were important to point out that: i) the mechanism in enhancement of S max /E max values was unclear and ii) the modification of A-site was more sensitive to S max /E max values than that of B-site.…”
Lead-free ceramics of composition (0.97 ¹ x)Bi 0.5 Na 0.4 K 0.1 TiO 3 -0.03BiAlO 3 -xBi 0.5 Li 0.5 TiO 3 (BNKTBA-xBLTO) were synthesized using solid state technique. The strong enhancements in ferroelectric and electric-field-induced strain were obtained. The electric-field-induced strain values were increased from 410 pm/V to 688 pm/V for 6 mol% BLTO-added which results from the phase transition from rhombohedral to tetragonal structure. The maximum spontaneous polarization increased from 26.5 µC/cm 2 to 30.8 µC/cm 2 for 4 mol% BLTO solid solution in BNKTBA and then decreased as BLTO was further added. We expect that this work could be helpful for further understanding the original enhancement in electrical field-induced strain in lead-free BNKT-based ceramics due to comparison between A-and B-site co-modifications.
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