“…3c). 10 In normal spinel, all the divalent metal ions are present in tetrahedral sites whereas the trivalent metal ions are present in Various methods have been used for the synthesis of spinel compounds like coprecipitation, 12 Sol-gel, 18 Solvothermal, 20 microemulsion, 21 Mechanical milling, 22 Plasma, 23 Flux growth, 24 Solid-phase, 25 Combustion, 26 Microwave hydrothermal, 27 Pechini method, 28 Template, 29 Electrospinning, 30 Thermal treatment, 31 Spray pyrolysis, 32 Aerosol, 33 Forced Hydrolysis, 34 Glycol-thermal, 35 refluxing, 36 and microwave-assisted method. 37 Spinels have attracted a lot of interest because of their numerous redox states, terrific electrochemical stability, and pseudocapacitive behavior, making them promising candidates for electrochemical sensing.…”