2016
DOI: 10.1007/s13197-016-2237-5
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Stability and microstructure of freeze-dried guava pulp (Psidium guajava L.) with added sucrose and pectin

Abstract: Freeze-dried guava pulp powders, formulated with the addition of sucrose (0-20 g/100 g pulp) and pectin (0-1.0 g/100 g pulp), were obtained, and their stability was evaluated with respect to the water adsorption isotherms, thermal analysis and microstructure. The GAB (Guggenheim-Anderson-de Boer), Peleg and BET (Brunauer-Emmett-Teller) models were used to evaluate the water adsorption. The microstructure was examined using optical microscopy with polarized light and scanning electron microscopy (SEM). The GAB … Show more

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Cited by 14 publications
(13 citation statements)
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References 29 publications
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“…In general, the particles exhibited varied and irregular shapes, besides presence of pores, indicated by the arrows in Figure 1, which are typical of lyophilized products. Conceição et al (2016) claim that powders obtained by lyophilization have a porous structure due to the solid state of water during the (1) by these agents, such as rounding of particle edges, reducing the segregation of the particles of the powders.…”
Section: Resultsmentioning
confidence: 99%
“…In general, the particles exhibited varied and irregular shapes, besides presence of pores, indicated by the arrows in Figure 1, which are typical of lyophilized products. Conceição et al (2016) claim that powders obtained by lyophilization have a porous structure due to the solid state of water during the (1) by these agents, such as rounding of particle edges, reducing the segregation of the particles of the powders.…”
Section: Resultsmentioning
confidence: 99%
“…This microstructure is quite different when compared to spray dried particles, which commonly exhibit spherical structures without fissures or cracks. In fact, the sublimation of water results in a rigid and porous structure with no shrinkage, which is characteristic of freeze dried samples (Conceição, Fernandes, & Resende, 2016).…”
Section: Scanning Electron Microscopy (Sem) and X-ray Diffractionmentioning
confidence: 99%
“…Above the glass transition temperature (Tg), the change from the more stable glassy state to the rubbery state occurs [14]. Freeze-dried fruit pulps, as sugar-rich foods, have a low Tg value in the range of 5-15 • C [15,16]. For this reason, they present collapse and other structural problems related to stickiness and caking, which begin to be developed about 20 • C above Tg [14].…”
Section: Introductionmentioning
confidence: 99%