Simultaneous Quantitation of Boric Acid and Calcium Fructoborate in Dietary Supplements by HPTLC-Densitometry

Biță, Andrei; Mogoşanu, George Dan; Bejenaru, Ludovic Everard; Oancea, Carmen Nicoleta; Bejenaru, Cornelia; Croitoru, Octavian; Rău, Gabriela; Neamțu, Johny; Scorei, Iulia Daria; Scorei, Ion Romulus; Hunter, John M.; Evers, Brad; Nemzer, Boris; Anghelina, Florin; Rogoveanu, Otilia-Constantina

doi:10.2116/analsci.33.743

Cited by 11 publications

(14 citation statements)

References 20 publications

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“…In order to prevent matrix interferences and/or to enhance sensitivity of a method some pretreatment procedures have been applied in most techniques before determination of boron. Most of the pretreatment procedures involve preconcentration and/or separation procedures such as solid phase extraction, liquid-liquid extraction, dispersive liquid-liquid microextraction, ion-exchange method and cloud-point extraction [17,24,42,43,59,[65][66][67][68][69].…”

Section: Discussionmentioning

confidence: 99%

“…Linear working range and LOD (S/N = 3) and reproducibility were found as 0.1 -50 ppm, 5 ppb and 5%, respectively. Bita et al [59] describe the simultaneous determination of boric acid (BA) and calcium fructoborate (CFB) in dietary supplements by a new high-performance thin-layer chromatographic (HPTLC) method. HPTLC silica gel G 60 F-254 precoated glass plates and 2-propanol-water 8:2 (v/v) were used as the stationary phase and mobile phase, respectively.…”

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A critical review on the determination of boron in various matrices

Türker¹

2019

Journal of Boron

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Boron is an element with a wide range of uses. Boron, which is the main component in boron minerals, is present as a minor component or even a trace component in other sources. Depending on the increase in the boron usage areas, the boron concentrations in environmental samples such as water, soil and air is also increasing. Therefore, it is important to determine boron in such samples accurately and precisely. In order to determine boron in various sample matrices, various analytical methods have been developed and used. This review focuses on the analytical methods for the determination of boron in various sample matrices. This review covers approximately the last four years (2015-August 2018), offering a critical review of the boron determination by various techniques.

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Section: Discussionmentioning

confidence: 99%

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confidence: 99%

A critical review on the determination of boron in various matrices

Türker¹

2019

Journal of Boron

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“…An aqueous 1 mg/mL stock solution of BA was prepared, while the concentration for the stock solution of CaFB was 5 mg/mL. The standard working solutions were obtained by diluting the stock solutions with water to achieve the concentration range of 0.2–0.6 μg/band for BA and 1–3 μg/band for CFB, respectively [ 18 ]. The samples were obtained by dissolving 20 mg of BA and CaFB hydrogels in 10 mL of water.…”

Section: ⧉ Materials and Methodsmentioning

confidence: 99%

Preclinical and histological study of boron-containing compounds hydrogels on experimental model of periodontal disease

Mitruț¹,

Cojocaru²,

Scorei³

et al. 2021

Rom J Morphol Embryol

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Periodontitis is a disease that affects a wide group of people, and there has been an increased interest in the research of finding useful materials that help reduce inflammation and the further loss of tissue. In this study, we have tested a boron-containing compound (BCC) Calcium Fructoborate (CaFB) and Boric Acid (BA) hydrogels on the gingival level on Wistar rats. First, we have induced the periodontal disease at the lower incisors, we have applied the hydrogels and after a week, we have euthanized the rats. Next, the oral soft tissue reaction was clinically and then histologically investigated. Our study has shown good clinical response of the oral tissue, and we have noticed lower levels of inflammation on the experimental groups treated with the BCCs hydrogels. Despite the generally good response of the biological structures to the presence of BA and CaFB on periodontal level, more scientifically proved information is needed to obtain the desired biological responses in all clinical situations.

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“…At regular time intervals, 0.5 mL of solution was taken and immediately replaced with an equal volume of PBS. The amount of released CaFb was determined by the high-performance thin-layer chromatography (HPTLC) method [ 14 ]. To confirm that the compound truly was CaFb, we eluted one of the bands from the sample directly into the mass spectrometer and we obtained the expected mass spectrum [ 6 ].…”

Section: ⧉ Materials and Methodsmentioning

confidence: 99%

Calcium fructoborate coating of titanium–hydroxyapatite implants by chemisorption deposition improves implant osseointegration in the femur of New Zealand White rabbit experimental model

Varut¹,

Melinte²,

Pîrvu³

et al. 2021

Rom J Morphol Embryol

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This is an open-access article distributed under the terms of a Creative Commons Attribution-NonCommercial-ShareAlike 4.0 International Public License, which permits unrestricted use, adaptation, distribution and reproduction in any medium, non-commercially, provided the new creations are licensed under identical terms as the original work and the original work is properly cited. ORIGINAL PAPERCalcium fructoborate coating of titanium-hydroxyapatite implants by chemisorption deposition improves implant osseointegration in the femur of New Zealand White rabbit experimental model RENATA-MARIA VĂRUŢ 1) , PETRU RĂZVAN MELINTE 2) , ANDREEA SILVIA PÎRVU 3) , OANA GÎNGU 4) , GABRIELA SIMA 4) , CARMEN NICOLETA OANCEA 5) , ALINA CRISTINA TEIŞANU 4) , GHEORGHE DRĂGOI 6) , ANDREI BIŢĂ 7,8) , HORIA OCTAVIAN MANOLEA 9) , IOANA MITRUŢ 3,9) , OTILIA CONSTANTINA ROGOVEANU 10) , ION ROMULUS SCOREI 8) , JOHNY NEAMŢU 11)

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Simultaneous Quantitation of Boric Acid and Calcium Fructoborate in Dietary Supplements by HPTLC-Densitometry

Cited by 11 publications

References 20 publications

A critical review on the determination of boron in various matrices

A critical review on the determination of boron in various matrices

Preclinical and histological study of boron-containing compounds hydrogels on experimental model of periodontal disease

Calcium fructoborate coating of titanium–hydroxyapatite implants by chemisorption deposition improves implant osseointegration in the femur of New Zealand White rabbit experimental model

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