Simultaneous determination of platinum group elements and rhenium mass fractions in road dust samples using isotope dilution inductively coupled plasma-tandem mass spectrometry after cation exchange separation

Mitra, Arijeet; Sen, Indra Sekhar; Walkner, Christoph; Meisel, Thomas

doi:10.1016/j.sab.2020.106052

Cited by 11 publications

(8 citation statements)

References 67 publications

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“…Research fields and objectives. The research fields of the above references covered biology, 1-15 energy, 16 environment, 9,[17][18][19][20][21][22][23][24][25][26][27][28][29][30][31][32] food/medical, 10-12,25-27,33-40 geology, 28,41-47 material, [48][49][50][51][52][53][54][55][56][57][58][59][60] and radionulide, 4,[22][23][61][62][63][64][65][66][67][68][69][70][71] respectively. In addition to these conventional elemental analysis topics, a study on the gas phase catalytic reaction has also been reported by using the reaction cell of ICP-QMS/QMS as the in-situ reaction field.…”

Section: References Investigatedmentioning

confidence: 99%

Trends and Advances in Inductively Coupled Plasma Tandem Quadruple Mass Spectrometry (ICP-QMS/QMS) With Reaction Cell

Zhu¹

2021

At.Spectrosc.

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Trends and advances in the development and application of inductively coupled plasma tandem quadrupole mass spectrometry (ICP-QMS/QMS) with a reaction cell is reviewed mainly based on publications from January 2018 to July 2021. ICP-QMS/QMS has been applied in various research fields covering the sciences of biology, energy, environmental, food/medical, geology, materials, and radionuclide. The objectives of analysis cover the determination of elemental concentration, ion-gas reaction, isotope analysis, single particle analysis, and chemical speciation analysis. Measurement of most elements in the periodic table are reported except for H, N, O, F, rare gas, and some of the radionuclides. In addition to the default reaction/collision gases (i.e., He, H2, O2, and NH3), N2O, CO2, CH4, CH3F, C2H4, and C2H6 have been used as reaction gases to improve the capability of separating spectral interferences or to study the ion-molecule reactions. Typical applications of ICP-QMS/QMS analysis in the major research fields are also discussed.

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Section: References Investigatedmentioning

confidence: 99%

Trends and Advances in Inductively Coupled Plasma Tandem Quadruple Mass Spectrometry (ICP-QMS/QMS) With Reaction Cell

Zhu¹

2021

At.Spectrosc.

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“…Measuring PGEs and Re at trace levels in road dust samples remains problematical because of severe isobaric and polyatomic interferences that can arise in ICP-MS analysis. In a new procedure, dust samples were digested 33 in inverse aqua regia in a HPA and the PGEs separated from the matrix by CEC for ID-ICP-MS/MS analysis. The use of a mass filter to select only ions of interest in conjunction with the use of ion-reaction chemistry meant that spectral interferences derived from residual elements remaining after clean-up could be avoided.…”

Section: Air Analysismentioning

confidence: 99%

“…The method was applied to seven surface soils from China and a sediment from Denmark. A key step 33 in a ID-ICP-MS/MS method for simultaneous determination of PGEs and Re was removal by CEC of the majority of elements likely to form isobaric or polyatomic ion interferences. The reaction gas in the collision cell was 10% NH 3 in He.…”

Section: Analysis Of Soils Plants and Related Materialsmentioning

confidence: 99%

Atomic spectrometry update – a review of advances in environmental analysis

Bacon

Butler

Cairns

et al. 2022

J. Anal. At. Spectrom.

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“…The ICP-MS/MS instrumentation has taken the conventional ICP-MS technology to the next level through its capability of interference-free elemental/isotopic determination of the majority of the elements in the periodic Mixed acid dissolution in HPA-S, matrix removal by cation-exchange column followed by ICP-MS/MS determination 43 .…”

Section: Conclusion and Futurementioning

confidence: 99%

“…In addition, severe isobaric and polyatomic interferences make their determination by conventional ICP-MS difficult. Mitra et al43 determined PGE and Re in road dust samples using ICP-MS/MS after sample decomposition by high-pressure asher (HPA) at a pressure of 130 bars and a PGE and Re from the sample matrix, and for complete removal of potentially interfering species arising from Cd, Hg, Zr, Hf, Mo, and W, and with isotope dilution (ID) as a calibration strategy. Table2presents the PGE and Re data obtained in a road dust reference sample and a base metal sulphide bearing komatiite sample in comparison with certified…”

mentioning

confidence: 99%

Inductively Coupled Plasma-Tandem Mass Spectrometry (ICP-MS/MS) and Its Applications

Balaram¹

2022

J. ISAS

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During the last about 10 years, the inductively coupled plasma tandem quadrupole mass spectrometry (ICP-MS/MS) technique with reaction cell is being utilized for the analyses of several trace elements/isotopes at very low concentration levels in a variety of matrices including geological, environmental, biological, medical, nuclear, agriculture, food, material and metallurgical sciences. Both solution nebulization, as well as direct analysis of samples by laser ablation (LA-ICP-MS/MS), are utilized for sample introduction. In fact, ICP-MS/MS technique with collision reaction cells eliminated the need for laborious chemical separations using methods such as ion-exchange or solvent extraction procedures to eliminate/minimize spectral and matrix interference effects as these interferences are removed using online chemical reactions within the instrument itself (chemical resolution). In addition, the technique is hyphenated with chromatographic techniques such as GC and HPLCfor a variety of applications. The detection limits for several elements in the periodic table lie in the pg/ml-fg/ml range, and the technique compares favourably with the expensive, complex, and superior high resolution-ICP-MS (HR-ICP-MS), both in terms of the detection limits as well as the ability to remove the most complex interferences. Thus, the ICP MS/MS made the determinations of elemental as well as isotopic concentrations very simple andeasy even in complex materials with several novel quantification approaches. This article provides an overview of these new developments during the last decade along with several applications in all areas of science and technology.

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Simultaneous determination of platinum group elements and rhenium mass fractions in road dust samples using isotope dilution inductively coupled plasma-tandem mass spectrometry after cation exchange separation

Cited by 11 publications

References 67 publications

Trends and Advances in Inductively Coupled Plasma Tandem Quadruple Mass Spectrometry (ICP-QMS/QMS) With Reaction Cell

Trends and Advances in Inductively Coupled Plasma Tandem Quadruple Mass Spectrometry (ICP-QMS/QMS) With Reaction Cell

Atomic spectrometry update – a review of advances in environmental analysis

Inductively Coupled Plasma-Tandem Mass Spectrometry (ICP-MS/MS) and Its Applications

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