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2015
DOI: 10.1016/j.jchromb.2015.02.016
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Simultaneous determination of phenylurea herbicides in yam by capillary electrophoresis with electrochemiluminescence detection

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Cited by 34 publications
(11 citation statements)
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References 23 publications
(26 reference statements)
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“…The electrophoretic separation was performed in NH 4 HCO 3 electrolyte (adjusted to pH 8.5) reaching LODs of 2 ppbs for both studied matrices. The analysis of widespread used phenylurea herbicides such as monuron, monolinuron and diuron has been accomplished by electrochemiluminescence (ECL) detection after CE separation . As extraction method, a matrix solid‐phase dispersion (MSPD) procedure was proposed, showing quantitative recoveries (90.0–99.2%), with very low variability (RSD < 3.2%).…”
Section: Toxins Contaminants Pesticides and Residuesmentioning
confidence: 99%
“…The electrophoretic separation was performed in NH 4 HCO 3 electrolyte (adjusted to pH 8.5) reaching LODs of 2 ppbs for both studied matrices. The analysis of widespread used phenylurea herbicides such as monuron, monolinuron and diuron has been accomplished by electrochemiluminescence (ECL) detection after CE separation . As extraction method, a matrix solid‐phase dispersion (MSPD) procedure was proposed, showing quantitative recoveries (90.0–99.2%), with very low variability (RSD < 3.2%).…”
Section: Toxins Contaminants Pesticides and Residuesmentioning
confidence: 99%
“…The reported recovery values for spiked samples ranged from 96 to 105%, and the LOD for the herbicide in juice and tomato was 2 ppb. In a separate report, the application of CE‐ECL was investigated to the analysis of yam samples for the detection of three phenylurea herbicides, namely monuron, monolinuron, and diuron . Separations were performed using 25 mM phosphate buffer at pH 8.0 as BGE and a CE instrument coupled with an ECL detector.…”
Section: Toxins Contaminants Pesticides and Residuesmentioning
confidence: 99%
“…Wang et al [ 58 ] used dichloromethane as extractant and C18-bonded silica as sorbent because its non-polar characteristic provided the best recovery (>90%) for three phenylurea herbicides in rice powders. The MSPD procedure was also developed to handle phenylurea herbicides in yam samples [ 59 ]. MSPD is more applicable to the pretreatment of solid samples rather than other sample pretreated techniques.…”
Section: Sample Pretreatment Techniquesmentioning
confidence: 99%
“…These analytes were well separated within 8 min with LODs of 0.1 μg/L for isoproturon and linuron, and 0.2 μg/L for diuron. A similar CE-enhanced chemiluminescence system has been applied to detect three phenylurea herbicides (monuron, monolinuron, and diuron) in yam samples [ 59 ].…”
Section: Pesticide Analysis Using Capillary Electrophoresismentioning
confidence: 99%