“…On the other hand, when the concentration of silver ions in solution decreased, this promoted the formation of irregular quasi-spherical gold/silver bimetallic nanoparticles. The results of Cheng et al [35] do not agree with the present study due to the different processes and compositions.…”
Section: Effect Of Seed Solution Amount On the Microstructurecontrasting
“…On the other hand, when the concentration of silver ions in solution decreased, this promoted the formation of irregular quasi-spherical gold/silver bimetallic nanoparticles. The results of Cheng et al [35] do not agree with the present study due to the different processes and compositions.…”
Section: Effect Of Seed Solution Amount On the Microstructurecontrasting
“…1b). Gold nanostars were prepared using a versatile, room-temperature, surfactant free, one-step method as reported previously [20]. Ascorbic acid, a weak reducing agent, was added quickly into the HAuCl 4 aqueous solution containing a small amount of AgNO 3 as the structure director.…”
“…The synthesis of large (>100 nm) star-shaped nanoparticles has been thoroughly studied. Both seed-growth [8] and seedless [7,9] methods are now well known. Compared to the seedless method, seed-growth allows slightly smaller nanoparticles to be obtained under identical conditions (pH, precursor ratio, temperature, and intensity of mixing).…”
Section: Introductionmentioning
confidence: 99%
“…As our understanding of the SERS mechanism developed, different researchers attempted to calculate and synthesize nanostructures with greater Raman enhancement, including star-shaped gold and silver nanoparticles. A number of works proposed ways of obtaining nanostars with different numbers of rays [6], the lengths of which can be varied by changing the molar ratio between reacting AgNO 3 and HAuCl 4 [7]. The synthesis of large (>100 nm) star-shaped nanoparticles has been thoroughly studied.…”
A way of synthesizing bimetallic gold/silver nanoparticles with in situ seeding initiated by the addition of sodium borohydride is proposed. The obtained nanoparticles are studied by means of transmission electron microscopy (TEM). Changes in the optical density spectra of the nanoparticles during their coagulation are investigated. The technique allows the rapid acquisition of nontoxic SERS-active nanoparticles with maximum SERS enhancement factor about 10 5 in the near infrared range for Raman shifts typical for biological objects such as bacterial cells and spores.
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