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P, Sanz L. Snake venomics. Strategy and applications. J Mass Spectrom 2007; 42: 1405. He MY, Chen H. Current mass spectrometry of synthetic polymer. Curr Org Chem 2007; 11: 909. Helmke SM, Duncan MW. Measurement of the NO metabolites, nitrite and nitrate, in human biological fluids by GC-MS. J Chromatogr B 2007; 851: 83. Herrmann AM, Ritz K, Nunan N, Clode PL, Pett-Ridge J, Kilburn MR, Murphy DV, O'Donnell AG, Stockdale EA. Nano-scale secondary ion mass spectrometry -A new analytical tool in biogeochemistry and soil ecology: A review article. Soil Biol Biochem 2007; 39: 1835. Luque-Garcia JL, Neubert TA. Sample preparation for serum/plasma profiling and biomarker identification by mass spectrometry. J Chromatogr A 2007; 1153: 259. Nelson BC. The expanding role of mass spectrometry in folate research. Curr Anal Chem 2007; 3: 219. Portier S, Bremier S, Walker CT. Secondary ion mass spectrometry of irradiated nuclear fuel and cladding: An overview. Int J Mass Spectrom 2007; 263: 113. Vogl J. Characterization of reference materials by isotope dilution mass spectrometry. J Anal Atom Spectrom 2007; 22: 475. Wiechert W, Schweissgut O, Takanaga H, Frommer WB. Fluxomics: Mass spectrometry versus quantitative imaging. Curr Opin Plant Biol 2007; 10: 323. Williamson LN, Bartlett MG. Quantitative liquid chromatography/time-offlight mass spectrometry. Biomed Chromatogr 2007; 21: 567. Wyttenbach T, Bowers MT. Intermolecular interactions in biomolecular systems examined by mass spectrometry. Annu Rev Phys Chem 2007; 58: 511. 2 INSTRUMENTAL TECHNIQUES & METHODS Alvarez PA, Ramaswamy HS, Ismail AA. Effect of high-pressure treatment on the electrospray ionization mass spectrometry (ESI-MS) profiles of whey proteins. Int Dairy J 2007; 17: 881. Andreev VP, Li LY, Cao L, Gu Y, Rejtar T, Wu SL, Karger BL. A new algorithm using cross-assignment for label-free quantitation with LC-LTQ-FT MS. J Proteome Res 2007; 6: 2186. Bereman MS, Muddiman DC. Detection of attomole amounts of analyte by desorption electrospray ionization mass spectrometry (DESI-MS) determined using fluorescence spectroscopy. J Am Soc Mass Spectrom 2007; 18: 1093. Borges CR. Concept for facilitating analyst-mediated interpretation of qualitative chromatographic-mass spectral data: An alternative to manual examination of extracted ion chromatograms. Anal Chem 2007; 79: 4805. Carreira RJ, Cordeiro FM, Moro AJ, Rivas MG, Rial-Otero R, Gaspar EM, Moura I, Capelo JL. New findings for in-gel digestion accelerated by high-intensity focused ultrasound for protein identification by matrix-assisted laser desorption ionization time-of-flight mass spectrometry. J Chromatogr A 2007; 1153: 291. Chambers E, Wagrowski-Diehl DM, Lu ZL, Mazzeo JR. Systematic and comprehensive strategy for reducing matrix effects in LC/MS/MS analyses. J Chromatogr B 2007; 852: 22. Charvat A, Abel B. How to make big molecules fly out of liquid water: Applications, features and physics of laser assisted liquid phase dispersion mass spectrometry. Phys Chem Chem Phys 2007; 9: 3335. Codrea MC, Jimenez CR, Heri...
P, Sanz L. Snake venomics. Strategy and applications. J Mass Spectrom 2007; 42: 1405. He MY, Chen H. Current mass spectrometry of synthetic polymer. Curr Org Chem 2007; 11: 909. Helmke SM, Duncan MW. Measurement of the NO metabolites, nitrite and nitrate, in human biological fluids by GC-MS. J Chromatogr B 2007; 851: 83. Herrmann AM, Ritz K, Nunan N, Clode PL, Pett-Ridge J, Kilburn MR, Murphy DV, O'Donnell AG, Stockdale EA. Nano-scale secondary ion mass spectrometry -A new analytical tool in biogeochemistry and soil ecology: A review article. Soil Biol Biochem 2007; 39: 1835. Luque-Garcia JL, Neubert TA. Sample preparation for serum/plasma profiling and biomarker identification by mass spectrometry. J Chromatogr A 2007; 1153: 259. Nelson BC. The expanding role of mass spectrometry in folate research. Curr Anal Chem 2007; 3: 219. Portier S, Bremier S, Walker CT. Secondary ion mass spectrometry of irradiated nuclear fuel and cladding: An overview. Int J Mass Spectrom 2007; 263: 113. Vogl J. Characterization of reference materials by isotope dilution mass spectrometry. J Anal Atom Spectrom 2007; 22: 475. Wiechert W, Schweissgut O, Takanaga H, Frommer WB. Fluxomics: Mass spectrometry versus quantitative imaging. Curr Opin Plant Biol 2007; 10: 323. Williamson LN, Bartlett MG. Quantitative liquid chromatography/time-offlight mass spectrometry. Biomed Chromatogr 2007; 21: 567. Wyttenbach T, Bowers MT. Intermolecular interactions in biomolecular systems examined by mass spectrometry. Annu Rev Phys Chem 2007; 58: 511. 2 INSTRUMENTAL TECHNIQUES & METHODS Alvarez PA, Ramaswamy HS, Ismail AA. Effect of high-pressure treatment on the electrospray ionization mass spectrometry (ESI-MS) profiles of whey proteins. Int Dairy J 2007; 17: 881. Andreev VP, Li LY, Cao L, Gu Y, Rejtar T, Wu SL, Karger BL. A new algorithm using cross-assignment for label-free quantitation with LC-LTQ-FT MS. J Proteome Res 2007; 6: 2186. Bereman MS, Muddiman DC. Detection of attomole amounts of analyte by desorption electrospray ionization mass spectrometry (DESI-MS) determined using fluorescence spectroscopy. J Am Soc Mass Spectrom 2007; 18: 1093. Borges CR. Concept for facilitating analyst-mediated interpretation of qualitative chromatographic-mass spectral data: An alternative to manual examination of extracted ion chromatograms. Anal Chem 2007; 79: 4805. Carreira RJ, Cordeiro FM, Moro AJ, Rivas MG, Rial-Otero R, Gaspar EM, Moura I, Capelo JL. New findings for in-gel digestion accelerated by high-intensity focused ultrasound for protein identification by matrix-assisted laser desorption ionization time-of-flight mass spectrometry. J Chromatogr A 2007; 1153: 291. Chambers E, Wagrowski-Diehl DM, Lu ZL, Mazzeo JR. Systematic and comprehensive strategy for reducing matrix effects in LC/MS/MS analyses. J Chromatogr B 2007; 852: 22. Charvat A, Abel B. How to make big molecules fly out of liquid water: Applications, features and physics of laser assisted liquid phase dispersion mass spectrometry. Phys Chem Chem Phys 2007; 9: 3335. Codrea MC, Jimenez CR, Heri...
The construction and electrochemical response characteristics of poly(vinylchloride) (PVC) membrane selective electrodes for the determination of distigmine (Ds) are described. The sensing membrane comprised an ion-pair based on distigmine phosphomolybdate (Ds-PM), distigmine phosphotungstate (Ds-PT), distigmine silicomolybdate (Ds-SM), distigmine silicotungstate (Ds-ST), distigmine tetraphenylborate (Ds-TPB), and distigmine reineckate (Ds-Rein) in a plasticized PVC matrix with dioctylphthalate (DOP). The influence of membrane composition on the electrodes' response was studied. The electrodes showed a fast, stable and Nernstian response over a wide distigmine concentration range 5.0 · 10 À7 -1 · 10 À2 mol L À1 with a slope of $30.5 ± 1.0 mV dec À1 . The response is independent of the pH of test solution within the range 3.8-10.5. The life span of the electrodes extends to at least 2 months without any considerable divergence in potential and has a fast response time of <15 s. The electrodes showed good selectivity towards distigmine with respect to large numbers of ions in batch and FIA systems. The electrodes have been applied to the determination of distigmine in pure solution, pharmaceutical compound and human urine. The dissolution profile for Ubretid tablets (5 mg/tablet) was studied.
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