The temperature dependence of the 24 GHz anomalous FMR transmission peak previously observed in nickel specimens has been studied over the range 4 to 300 K using nickel single crystals deposited electrolytically on copper single crystal substrates. The experimental results have been compared with a calculation which includes magneto-elastic coupling between the lattice and the magnetization. In general, the theory gives a good account of the observed lineshapes and amplitudes, and an estimate can be made of the phonon mean free path and its temperature dependence.