Abstract:Improving the wear resistance of the surface of metal parts used in various industries is one of the relevant areas of materials science. The aim of this work was a comparative study of the wear resistance of a sample of an aluminum alloy (EN AW-2024, an aluminum alloy of the Al-Cu-Mg system) modified with ultrafine particles of minerals using the sclerometry method, which makes it possible to measure the physicomechanical properties of the material at the microscale, as well as determining some tribological p… Show more
“…To get reasonable results the test methods should be as close as possible to the actual operating conditions. In this regard, sclerometry provides rather limited information about the real tribological properties of the material, since the conditions for the formation of secondary structures are completely different from the real ones [21,48].…”
In this work, aluminum multicomponent alloys were studied after friction with steel in a mixed lubrication regime. The resulting secondary structures on the friction surface were investigated by scanning electron microscopy (SEM), energy dispersive analysis (EDX), X-ray photoelectron spectroscopy (XPS), and X-ray diffraction analysis (XRD). In addition to the mass transfer of steel counterbody particles, phase transformations and new chemical compounds formed as a result of interaction with the lubricant were revealed. The release of elements, mainly magnesium and to a lesser extent zinc, from a solid solution of aluminum alloy was also observed, which indicates the occurrence of a non-spontaneous reaction with a negative entropy production.
“…To get reasonable results the test methods should be as close as possible to the actual operating conditions. In this regard, sclerometry provides rather limited information about the real tribological properties of the material, since the conditions for the formation of secondary structures are completely different from the real ones [21,48].…”
In this work, aluminum multicomponent alloys were studied after friction with steel in a mixed lubrication regime. The resulting secondary structures on the friction surface were investigated by scanning electron microscopy (SEM), energy dispersive analysis (EDX), X-ray photoelectron spectroscopy (XPS), and X-ray diffraction analysis (XRD). In addition to the mass transfer of steel counterbody particles, phase transformations and new chemical compounds formed as a result of interaction with the lubricant were revealed. The release of elements, mainly magnesium and to a lesser extent zinc, from a solid solution of aluminum alloy was also observed, which indicates the occurrence of a non-spontaneous reaction with a negative entropy production.
“…For example, changing only some technological regimes using the technology of mineral coatings [1], which ensure that microparticles of minerals enter the metal, it is possible to obtain modified layers of various roughness Ra (average roughness) on structural steel samples, differing by almost an order of magnitude [2]. The interest in modified layers enriched with microparticles of minerals is due to their prospects as wear-resistant and/or antifriction coatings on the surfaces of friction pairs of various metals -steels [1], titanium [3], aluminum [4] operating in an aggressive environment -abrasive, marine water, in the presence of gases, acid solutions, under thermocyclic loads [5,6]. Studies show that the thickness of the modified layer, the coefficient of friction, the hardness of the layers depend both on the composition of the mineral mixtures and on the modes of particles entering the metal and the properties of the modified metal surface.…”
Section: Introductionmentioning
confidence: 99%
“…There are common problems for all methods in determining the hardness of thin layers and coatings, such as the effect of the substrate, surface roughness, and the presence of residual stresses, which can make a significant correction in the measurement results [4]. For example, the influence of the base metal substrate in measuring hardness consists in the fact that the recorded response of the material during measurement depends on the modified layer and on the properties of the metal volume [13].…”
One of the important characteristics of the surface properties of metal parts subjected to friction is hardness. Hardness measurements are important for determining the operational characteristics of parts and monitoring the technological regimes of surface modification. However, hardness measurements of thin modified layers made by different methods can lead to differences in measurement results. The aim of the article was to study the hardness of a metal surface modified with ultrafine particles of minerals by two different methods (instrumental indentation and Vickers hardness measurement) and a comparative analysis of the measurement results obtained by these methods.Standard Vickers hardness measurements at loads of 0.025, 0.1 and 0.5 kgf showed a qualitative difference between the hardness values of the two samples modified with different mixtures of ultrafine particles of minerals and a large heterogeneity of the hardness values over the area. By the method of instrumental hardness, standard measurements were performed without preliminary selection of the indentation site (at a load of 1.05 N) and measurements during indentation into even sections (at low loads of 10 mN).It is noted that the high precision of measurements implemented by instrumental indentation, due to the large roughness of the samples, leads to large values of the error in calculating the measurement results. An additional difference in the results of measurements performed by two methods at shallow indentation depths may be due to the fact that the object under study has a complex structure consisting of a metal matrix and particles distributed over the depth of the sample. A possible way out of the situation lies in the transition from the use of hardness measures when calibrating instruments to standard samples of properties for which the constancy of mechanical properties in the measured range of indentation depths will be ensured, but which are not yet available in research practice. Therefore, at present, when carrying out work related to the search for optimal conditions for obtaining thin wear-resistant layers on the surface of metals modified with ultrafine particles of minerals, comparative measurements performed by one measurement method are recommended.
“…One of the types of technologies currently developing surface hardening of a metal surface is the socalled technology of mineral coatings [6]. The essence of the technology is to create a modified surface layer with a thickness of 5-30 microns by plastic deforming it with the help of ultrasonic and mechanical effects that activate the incorporation of ultrafine mineral particles into the bulk of the metal [7,10]. The modification of the surface of a metal part is carried out at room temperature, locally, without the use of vacuumized space, baths, furnaces, which gives the technology additional marketing advantages [6][7][8].…”
Section: Introductionmentioning
confidence: 99%
“…The basic procedure for modifying the surface of a metal according to the technology of mineral coatings consists of four stages [6,7]: electrospark surface treatment; surface texturing; the introduction of ultrafine particles into the surface layer using an ultrasound unit; use of ball and roller knurling in surface treatment. As a result, a surface layer is formed that has high antifriction, wearresistant, extreme-pressure properties [8][9][10]. Another part of the technology is mixtures of ultrafine minerals, the particles of which are introduced into the surface space using some of these methods.…”
The results of testing sets of samples of a nipple coupling with a threaded connection NC-50 (4 ½ IF) of API 7 standard of pipes made of X 3 MnCrNiMoN 20 13 steel with a wear-resistant mineral coating and without coating are presented. A set of samples of a nipple-coupling pipe made of X 3 MnCrNiMoN 20 13 steel with a wear-resistant mineral coating successfully withstood the planned number of screwing and unscrewing cycles (400 cycles), which is more than an order of magnitude more than a set of samples of this steel without mineral coating (30 cycles). The predicted number of cycles of screwing and unscrewing this pair is not less than 1000.
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