Report for 2011 on the results from the monitoring of veterinary medicinal product residues and other substances in live animals and animal products

,

doi:10.2903/sp.efsa.2013.en-363

Cited by 5 publications

(2 citation statements)

References 5 publications

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“…Until now, all samples tested with this method have been qualified as compliant with the specified requirements. Based on the European Food Safety Authority (EFSA)'s published reports summarising the monitoring results in EU Member States, it can be concluded that until now only one noncompliant result for STAN was found in cattle in 2011 in Italy (19). Despite the low percentage of noncompliant results in the EU over the years, ongoing monitoring of residues of banned compounds is justified; therefore, analytical methods in laboratories should be constantly improved to ensure the safety and health of food consumers.…”

Section: Discussionmentioning

confidence: 99%

Liquid chromatographytandem mass spectrometry methods for determination of stanozolol and l6β-hydroxy-stanozolol in animal urine

Matraszek-Źuchowska,

Kłopot,

Sielska

et al. 2023

Journal of Veterinary Research

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Introduction Because of the activities and effects they induce, hormones are prohibited for use for anabolic purposes in farm animals intended for slaughter, which is regulated in the European Union by relevant legal provisions. Therefore, there is an obligation to monitor residues of hormones in animals and food of animal origin to ensure consumer safety. A hormone banned but used formerly for fattening cattle, stanozolol, and its metabolite 16β-OH-stanozolol are synthetic compounds that belong to a large group of steroid hormones. This study investigates residues of these compounds in animal urine. Material and Methods From 2006–2022, 2,995 livestock urine samples were tested for stanozolol residues in Poland as part of the National Residue Monitoring Programme. A liquid chromatography–tandem mass spectrometry method to determine stanozolol and 16β-OH-stanozolol in animal urine was developed and validated according to the required criteria. Urine sample analysis was based on enzymatic hydrolysis of hormones potentially present in it to the free form, extraction of them from the sample with a mixture of n-hexane and butyl alcohol, purification of an extract on an NH2 amine column and finally, instrumental detection. Results The apparent recovery and precision parameters of the developed method were in line with the established criteria, while its decision limits CCα and detection capabilities CCβ were lower than the recommended concentration for analytical purposes set at 2 μg L−1 (valid until December 15, 2022; currently set as 0.5 μg L−1). Conclusion All examined samples were compliant with the evaluation criteria.

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Section: Discussionmentioning

confidence: 99%

Liquid chromatographytandem mass spectrometry methods for determination of stanozolol and l6β-hydroxy-stanozolol in animal urine

Matraszek-Źuchowska,

Kłopot,

Sielska

et al. 2023

Journal of Veterinary Research

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“…The defined missions in Codex Alimentarius [16,17] were tracked to create a HACCP plan for all of the predicted hazards (in pastrami manufacturing) that comprise the subsequent seven rules of the HACCP system, namely: R1: Perform hazard analysis (HA); R2: Distinguish critical control points (CCP); R3: Entrench critical limits (CL); R4: Supervise each CCP; R5: Reside corrective action; R6: Demonstrate verification procedures; R7: Record keeping. The implementation of the HACCP safety system was based on the passage and development of the successively and complementary stages that were previously mentioned.…”

Section: Methodsmentioning

confidence: 99%

Hazard Analysis and Critical Control Point (HACCP) Application to Dry-Cured Pastrami in Egyptian Pastrami Factories

El-Mougy,

Abd-Elghany,

Imre

et al. 2023

Foods

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The current study established a HACCP tactic for all hazards related to Egyptian dry-cured pastrami production. All types of hazards that could occur at each production step were depicted. The fabrication steps of pastrami were originally based on the processes and conclusions presented in two previous publications by members of the research team; thus, the current scientific paper is considered a completion of the two previous publications. All operations executed and products manufactured outside the pastrami factory were excluded. The HACCP system was only applied to dry-cured pastrami production stages from receiving frozen raw meat and non-meat ingredients until packaging and storing the final product. Four CCPs were detected and taken into account. The permissible critical limits of additives and non-meat ingredients were considered. Suitable corrective actions were arranged. Regular HACCP plan review, proper recording of detected CCPs and critical limits were necessary for validation processes. Following up with the supply chain by obtaining the certified suppliers, together with the importance of the verification procedures of the elaborated HACCP plan, were essential in order to ensure the production of safe food without defects.

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Simultaneous Determination of Nine Sulphonamides by LC-MS for Routine Control of Raw Honey Samples

et al. 2016

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Report for 2011 on the results from the monitoring of veterinary medicinal product residues and other substances in live animals and animal products

Cited by 5 publications

References 5 publications

Liquid chromatographytandem mass spectrometry methods for determination of stanozolol and l6β-hydroxy-stanozolol in animal urine

Liquid chromatographytandem mass spectrometry methods for determination of stanozolol and l6β-hydroxy-stanozolol in animal urine

Hazard Analysis and Critical Control Point (HACCP) Application to Dry-Cured Pastrami in Egyptian Pastrami Factories

Simultaneous Determination of Nine Sulphonamides by LC-MS for Routine Control of Raw Honey Samples

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