Rapid high-performance liquid chromatographic determining technique of sulfamonomethoxine, sulfadimethoxine, and sulfaquinoxaline in eggs without use of organic solvents

Furusawa, Naoto

doi:10.1016/s0003-2670(03)00080-1

Cited by 58 publications

(28 citation statements)

References 14 publications

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“…The continual overuse of sulfonamides, much attention has been paid to their potential carcinogenesis and the worry of the development of antibacterial resistance. Because of these health concerns, the European Commission (EC), America and other countries, for example China, have adopted a maximum acceptable limit of residual sulfonamide in foods of animal origin, for example meat, milk and eggs [3]. Therefore, there is a constant requirement for good analytical protocols based on efficient analytical processes (sensitive, selective, fast and inexpensive) by legislation, health authorities and companies operating in the food market.…”

Section: Introductionmentioning

confidence: 99%

Synthesis and characterization of the core–shell magnetic molecularly imprinted polymers (Fe3O4@MIPs) adsorbents for effective extraction and determination of sulfonamides in the poultry feed

Kong

Gao

et al. 2012

Journal of Chromatography A

237

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Section: Introductionmentioning

confidence: 99%

Synthesis and characterization of the core–shell magnetic molecularly imprinted polymers (Fe3O4@MIPs) adsorbents for effective extraction and determination of sulfonamides in the poultry feed

Kong

Gao

et al. 2012

Journal of Chromatography A

237

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“…Examples of applications include sulphonamides in milk [19,[132][133][134], eggs [132,135,136], plasma [137] and edible tissues [138,139], benzimidazoles in milk [19], tetracyclines in egg [140], β-agonist in urine [141], penicillin G in muscle, kidney and liver [142], and spiramycin (a macrolide) in egg and chicken muscle [143].…”

Section: Ultra-filtrationmentioning

confidence: 99%

Current trends in sample preparation for growth promoter and veterinary drug residue analysis

Kinsella

O’Mahony

Malone

et al. 2009

Journal of Chromatography A

175

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A comprehensive review is presented on the current trends in sample preparation for isolation of veterinary drugs and growth promotors from foods. The objective of the review is to firstly give an overview of the sample preparation techniques that are applied in field. The review will focus on new techniques and technologies, which improve efficiency and coverage of residues. The underlying theme to the paper is the developments that have been made in multi-residue methods and particularly multi-class methods for residues of licensed animal health products, which have been developed in the last couple of years. The role of multi-class methods is discussed and how they can be accommodated in future residue surveillance.

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“…3, 2011 technique of analysis. There are methods that use high performance liquid chromatography (HPLC) with fluorescence detector, [2][3][4][5][6] or with ultra-violet (UV) detector, [7][8][9][10] or else with diode array detector (DAD), [11][12][13][14][15][16][17][18][19][20][21][22][23][24][25][26][27] but mass spectrometer (MS) detectors are the most appropriate because they give enough information for molecular identification.…”

Section: Introductionmentioning

confidence: 99%

Development and validation of analytical method for sulfonamide residues in eggs by liquid chromatography Tandem Mass Spectrometry based on the Comission Decision 2002/657/EC

Cruz¹,

Soares²,

Marques³

et al. 2011

J. Braz. Chem. Soc.

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A técnica de cromatografia líquida acoplada a um espectrômetro de massas com ionização "electrospray" (LC-ESI-MS/MS) foi usada para a determinação simultânea de resíduos de dez sulfonamidas (SAs: sulfacetamida, sulfatiazol, sulfamerazina, sulfametazina, sulfametoxipiridazina, sulfametazol, sulfacloropiridazina, sulfametoxazol, sulfadimetoxina e sulfaquinoxalina) em ovos. As amostras foram preparadas por precipitação das proteínas com acetonitrila seguida por extração em fase sólida. Após remoção do solvente e reconstituição, os extratos finais foram injetados no LC-ESI-MS/MS no modo positivo para todas as sulfonamidas. O método validado resultou em recuperação entre 87 e 116% com desvios padrão relativo entre 8,5 e 27,2%, CCa entre 101,0 e 122,1 ng g -1 e CCb entre 114,5 e 138,8 ng g -1 . O método analítico, no qual foram utilizadas amostras fortificadas, foi validado baseado na Decisão da Comissão 2002/657/CE.Liquid chromatography-electrospray ionization -tandem mass spectrometry (LC-ESI-MS/MS) was used to simultaneous determination of ten sulfonamide (SAs) residues (sulfacetamide, sulfathiazole, sulfamerazine, sulfamethazine, sulfamethoxypyridazine, sulfamethizole, sulfachloropyridazine, sulfamethoxazole, sulfadimethoxine and sulfaquinoxaline) in eggs. Samples were extracted with acetonitrile and the supernatants were cleaned up by solid phase extraction. After solvent evaporation and reconstitution, aliquots of the final extracts were injected into a LC-ESI-MS/MS in positive mode for all sulfonamides. The validated method resulted in recoveries ranging between 87 and 116% with relative standard deviations between 8.5 and 27.2%, CCa between 101.0 and 122.1 ng g -1 , and CCb between 114.5 and 138.8 ng g -1 . The analytical method, using fortified samples, was validated based on the Commission Decision 2002/657/EC.

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Rapid high-performance liquid chromatographic determining technique of sulfamonomethoxine, sulfadimethoxine, and sulfaquinoxaline in eggs without use of organic solvents

Cited by 58 publications

References 14 publications

Synthesis and characterization of the core–shell magnetic molecularly imprinted polymers (Fe3O4@MIPs) adsorbents for effective extraction and determination of sulfonamides in the poultry feed

Synthesis and characterization of the core–shell magnetic molecularly imprinted polymers (Fe3O4@MIPs) adsorbents for effective extraction and determination of sulfonamides in the poultry feed

Current trends in sample preparation for growth promoter and veterinary drug residue analysis

Development and validation of analytical method for sulfonamide residues in eggs by liquid chromatography Tandem Mass Spectrometry based on the Comission Decision 2002/657/EC

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