1993
DOI: 10.1093/jaoac/76.4.735
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Rapid Determination of Supplemental Vitamin E Acetate in Feed Premixes by Capillary Gas Chromatography

Abstract: A rapid capillary gas chromatographic method was developed for determination of supplemental cc-tocopherol acetate (containing and verified at 50–5000 mg/kg feed) in various kinds of feed premixes. The method is based on simple n-hexane extraction of feed samples pretreated with a solution of acetic acid in ether for matrix breakdown followed by column cleanup on deactivated alumina to eliminate background interference. Fused silica chromatography is completed in 3 min. The withinday precision expressed as the… Show more

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Cited by 10 publications
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“…The extraction process used (31) is a modification of Kmostak`s method (34), by incorporation of ultrasound treatment instead of agitation. The analytical determination was carried out in a gas chromatography (CG-FID) -Fisons Instrument model NPD 800.…”
Section: Methodsmentioning
confidence: 99%
“…The extraction process used (31) is a modification of Kmostak`s method (34), by incorporation of ultrasound treatment instead of agitation. The analytical determination was carried out in a gas chromatography (CG-FID) -Fisons Instrument model NPD 800.…”
Section: Methodsmentioning
confidence: 99%
“…Para la extracción de las vitaminas E y D se utilizó el método descrito por Kmostak (1993) (24) modificado por Cortes (2004) (25). La extracción de la vitamina B 9 y C se basaron según las metodologías propuestas por Arcot y Shrestha (2005) (26), y por Gutiérrez et al (2007) (27), respectivamente.…”
Section: Extracción Y Cuantificación De Cfaunclassified
“…Las frutas frescas e impregnadas fueron sometidas a un procedimiento de extracción y cuantificación de la vitamina E, según el método de Kmostak y Kurtz, 1993 (22), modificado por Cortés, 2004 (23). La cuantificación de la vitamina E se determinó por cromatografía líquida de alta resolución (HPLC) en un equipo Agilent 1100.…”
Section: Extracción Y Cuantificación De Vitamina Eunclassified