Purification of Plutonium Sulfate Tetrahydrate by Recrystallization and Ion Exchange.

Wenzel, A.W.; Pietri, C.E.

doi:10.1021/ac60202a073

Cited by 5 publications

(1 citation statement)

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“…Commercial databases searched include Thermo Fisher Scientific's Fisher Scientific, Merck's Mil-liporeSigma, and Avantor's VWR. To compile a more inclusive list of precursor metal salts, a literature search was conducted using Clarivate's Web of Science Group database [16][17][18][19][20][21][22][23][24][25][26][27][28][29][30]. Searches included the name of the metal element and the salt compound, such as "lithium nitrate," for every element and salt.…”

Section: Precursor Data Collection Methodsmentioning

confidence: 99%

Complex Oxide Nanoparticle Synthesis: Where to Begin to Do It Right?

2022

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Synthesis of advanced ceramics requires a high degree of control over the particle size and stoichiometry of the material. When choosing a synthesis method for complex oxides it is important to begin with the correct precursors and solvents to achieve high purity nanoparticles. Here, we detail the selection process for precursors and solvents for liquid-phase precipitation synthesis. Data for metal nitrate, chloride, acetate, and oxalate precursors has been compiled to assist future synthesis. The role of hydration within the precursors is discussed as it affects the final stoichiometry of the material. Melting temperatures are also compiled for these compounds to assist in material selection. The solubility of the precursors in different solvents is examined to determine the correct solvent during synthesis. As an example, using the methodology presented here, two different materials are synthesized based on commonly available precursors. A catalyst based on a quaternary perovskite and an advanced ionic conductor based on a high entropy fluorite oxide are synthesized using precipitation methods and their characterization is detailed.

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