Production Support and Process Control of PV Materials by Direct Sampling High-Resolution Glow Discharge Mass Spectrometry Methods

Hockett, R. S.; Kasik, Martin; Putyera, Karol; Michellon, C.

doi:10.4229/23rdeupvsec2008-3av.1.50

23rd European Photovoltaic Solar Energy Conference and Exhibition 2008

DOI: 10.4229/23rdeupvsec2008-3av.1.50

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Production Support and Process Control of PV Materials by Direct Sampling High-Resolution Glow Discharge Mass Spectrometry Methods

R. S. Hockett¹,

Martin Kasik²,

Karol Putyera³

et al.

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Quantification of Trace and Ultra-trace Elements in Nuclear Grade Manufactured Graphites by Fast-Flow Glow Discharge Mass Spectrometry and by Inductively Coupled Plasma – Mass Spectrometry after Microwave – Induced Combustion Digestions

et al. 2009

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Fast-Flow Glow Discharge Mass Spectrometry (FF-GDMS) and Inductively Coupled Plasma -Mass Spectrometry after Microwave -Induced Combustion Digestions (MIC-ICP-MS) methods were developed for the determination of mg/kg-and µg/kg-level B, Mg, Al, Ca, Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Zr, Mo, Sb, W and Pb in nuclear-grade graphite. Consistent results have been achieved in determining trace elements like B, Ti, Cr, Mn, Zr, Sb and Pb by both methods, which vary mostly less than ±30%, and are in line with the manufacturer reference values. On Mg, Al, Fe, Co, Zn, Mo and W, FF-GDMS analyses also show good agreement with the manufacturer's data. Continuing efforts in identifying source of interference, which has limited the MIC-ICP-MS analysis of these elements, is currently underway.

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Quantification of Trace and Ultra-trace Elements in Nuclear Grade Manufactured Graphites by Fast-Flow Glow Discharge Mass Spectrometry and by Inductively Coupled Plasma – Mass Spectrometry after Microwave – Induced Combustion Digestions

et al. 2009

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Production Support and Process Control of PV Materials by Direct Sampling High-Resolution Glow Discharge Mass Spectrometry Methods

Cited by 1 publication

References 0 publications

Quantification of Trace and Ultra-trace Elements in Nuclear Grade Manufactured Graphites by Fast-Flow Glow Discharge Mass Spectrometry and by Inductively Coupled Plasma – Mass Spectrometry after Microwave – Induced Combustion Digestions

Quantification of Trace and Ultra-trace Elements in Nuclear Grade Manufactured Graphites by Fast-Flow Glow Discharge Mass Spectrometry and by Inductively Coupled Plasma – Mass Spectrometry after Microwave – Induced Combustion Digestions

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