“…The second weight loss in the range of 200–400 °C (10.63%) arose from the removal of bound water and the expulsion of dopant. The third weight loss in the range of 400–600 °C (3.11%) was due to the chemical decomposition of PANI chains . In the cases of the MBT–PANI–CeO 2 and PAA–MBT–PANI–CeO 2 pigments, the appearance of sharp peaks in the range of 230–400 °C showed the oxidative decomposition of PAA, PANI, and MBT .…”
“…The second weight loss in the range of 200–400 °C (10.63%) arose from the removal of bound water and the expulsion of dopant. The third weight loss in the range of 400–600 °C (3.11%) was due to the chemical decomposition of PANI chains . In the cases of the MBT–PANI–CeO 2 and PAA–MBT–PANI–CeO 2 pigments, the appearance of sharp peaks in the range of 230–400 °C showed the oxidative decomposition of PAA, PANI, and MBT .…”
“…Among these rare-earth conversion films, films containing cerium or lanthanum ions are pervasive and their anti-corrosion properties and applications as pretreatment layers have been widely researched (Aldykewicz et al, 1995;? ;Wang et al, 2004;Kumar et al, 2012). Figure 5 gives the schematic diagram of kinetics of the cerium-based film formation (Sun et al, 2019;Li et al, 2020).…”
“…At 1743cm -1 this is due to C=O stretching vibrations which is may be caused by carboxylic group of cadmium acetate is used in reaction [13]. The band at 1645, 1546, 1533 and 1516 cm -1 are due to NH2 bending vibrations which may be due to residue thiourea is used in reaction [13].The medium to strong bands of Cd-S stretching appears at 412 cm -1 and 650cm -1 [15]. …”
The nanocrystalline CdS powder was prepared using sol-gel method. The polyaniline were prepared using chemical oxidative polymerization of aniline. The PANI-CdS nanocomposites had been prepared via same method of polyaniline preparation and different concentrations of CdS (10, 20, 30, 40 and 50 wt%) were added. X-ray diffraction shows that the peaks of emeraldine salt polyaniline powder are located at 2θ = 21.
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