“…The increased temperature ramped to 230 °C at the rate of 3 °C/min, finally ramped to 310 °C at the rate of 10 °C/min, and held for 5 min” [ 308 ] | Therapeutic tea | 17 | 0.4–5.1 | Spiked samples: 89.9–102.2 | | <12 | GC-ECD: “Splitless, the initial oven temperature was 150 °C and was increased to 280 °C at 6 °C/min, RT 22 min” | [ 309 ] |
Tea | 20 | 0.16–2.06 | 0.54–3.84 | 80–94 | 2.43–2.93 | GC-MS: “The column temperature programs s were as the following: 70 °C (2 min), 150 °C (25 °C/min), 200 °C (3.0 °C/min), 280 °C (9.0 °C/min), isotherm (10 min), the total run time for the OCPs was 40.8. 70 °C (1.2 min) and the ramp rate was 10 °C/min to 280 °C (18 min)” | [ 310 ] |
Tea | 9 | 60–720 | 30–2400 | 75.87–111.56 | 0.8–9.0 | GC-ECD: “Oven temperature program was: initial temperature of 80 °C, ramped at 30 °C/min to 180 °C, ramped at 3 °C/min to 205 °C, held for 4 min, ramped at 20 °C/min to 290 °C, held for 8 min, ramped at 50 °C/min to 325 °C. The total GC run time was 27.92 min” | [ 269 ] |
Tea | 13 | 1.4–7.2 | | 86.1–100.3 | 3.1–11 | GC-MS: “The initial temperature was 50 °C, which was increased to 180 °C at 10 °C/min and maintained for 4 min. |
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