Pigment palette study of the XIX century plafond painting by Raman spectroscopy

Петрова, О. И.; Pankin, Dmitrii; Povolotckaia, Anastasia; Borisov, E. N.; Krivul’ko, Timur; Kurganov, Nikolai; Курочкин, А. В.

doi:10.1016/j.culher.2018.11.010

Cited by 31 publications

(17 citation statements)

References 16 publications

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“…Detection of Cu and Cl was caused by a coverage of small particles of green pigment. Vibration at 1051 cm −1 can be attribute to the absorption of lead white [33][34][35] (Fig. 3-white).…”

Section: Microscopic Observation Of Pigmentsmentioning

confidence: 97%

Characterization of a Mahamayuri Vidyarajni Sutra excavated in Lu’an, China

et al. 2019

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Historically, sutras played an important role in spreading Buddhist faith and doctrine, and today these remain important records of Buddhist thought and culture. A Mahamayuri Vidyarajni Sutra with polychrome paintings was found inside the cavity on top of the Nanmen Buddhist pagoda, built in the early Tang dynasty (618-627 CE) and located in Anhui Province, China. Textile was found on the preface which is strongly degraded and fragile. Unfortunately, the whole sutra is under severe degradation and is incomplete. Technical analysis based on scientific methods will benefits the conservation of the sutra. Optical microscopy (OM), micro-Raman spectroscopy combined with optical microscope (Raman), scanning electron microscopy in combination with energy dispersive X-ray analysis (SEM-EDS) and Fourier Transform Infrared Spectroscopy (FTIR) were used to characterize the pigment and gilded material, as well as the paper fiber and textile. Pigments such as cinnabar, minium, paratacamite, azurite, lead white were found. Gilded material was identified as gold. A five-heddle warp satin, made of silk, was found as the textile on the preface of the sutra. The sutra's preface and inner pages were made of paper comprised of bamboo and bark. As a magnificent yet recondite treasure of Buddhism, the sutra was analyzed for a better understanding of the material. A conservation project of the sutra will be scheduled accordingly.

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Section: Microscopic Observation Of Pigmentsmentioning

confidence: 97%

Characterization of a Mahamayuri Vidyarajni Sutra excavated in Lu’an, China

et al. 2019

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“…The samples of M4 were analyzed by micro-Raman. There were two noticeable Raman peaks at 417 and 1052 cm −1 , which corresponds to reported characteristic Raman peaks of lead-white (2PbCO 3 •Pb(OH) 2 ).The peak at 1052 cm −1 was the complete symmetric vibration of ν 1 , and at peak around 165, 417 cm −1 were the Pb-O band vibration [19].…”

Section: White Pigmentmentioning

confidence: 60%

“…For azurite pigment, the bands found in the spectral interval 0-600 cm −1 , were attributed to the Cu-O band vibration. the bands found in the spectral interval the 600-1400 cm −1 belongs to the carbonate group vibration [19]. At near 1095 cm −1 band was caused by the symmetric ν 1 CO 3 2− vibration of azurite [20].…”

Section: Blue Pigmentmentioning

confidence: 91%

“…The near 259 cm −1 band was the ν 2 bending vibration of S 3− ions and near 549 cm −1 bands was ν 1 , a symmetric stretching vibration of S 3− ions [19]. Under horizontal polarized light in Figure 5c, The pigment particles of M2 sample (azurite) were smaller in the range of 10-25 µm, the pigment particles were pale blue; however, some of them were green, which may be malachite.…”

Section: Blue Pigmentmentioning

confidence: 93%

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Investigation of Ancient Architectural Painting from the Taidong Tomb in the Western Qing Tombs, Hebei, China

Teri

et al. 2020

Coatings

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The Taidong Tomb in the imperial tombs of the Qing dynasties has great aesthetic value and a rich history. In this study, we conducted the first investigation ever performed on the raw materials used in the paintings in the Taidong Tomb. Energy dispersive X-ray spectroscopy (EDX), polarized light microscopy (PLM), X-ray diffraction (XRD), micro-Raman spectroscopy (m-RS), Fourier-transform infrared spectroscopy (FTIR) and pyrolysis–gas chromatography–mass spectrometry (Py-GC/MS) were used to comprehensively analyze the painting of Long’en Hall, Xipei Hall and the ceiling of Minglou. In the conclusion of the study, the paintings were found to contain natural mineral and synthetic pigments, including atacamite (Cu2Cl(OH)3), azurite (2CuCO3·Cu(OH)2), vermilion (HgS), carbon black (C)，anglesite (PbSO4), white lead (2PbCO3·Pb(OH)2), synthetic emerald green (Cu(CH3COO)2·3Cu(AsO2)2) and ultramarine ((Na,Ca)8(AlSiO4)6(SO4,S,Cl)2). This allows us to conclude that some of the architectural paintings were repainted in the mid-to-late 19th century. The mortar layer may consist of brick ash (albite, gismondine), lime water, tung oil and flour. The fiber layer material may be ramie. Researching the raw materials of the paintings in the Taidong Tomb is of great value because it provides scientific data for the future preservation of the paintings in the tomb.

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“…Комбинации этих методов, а также дополнение их другими структурными методами, например, рентгеновскими (рентгеновская дифракция, рентгенофлуоресцентный анализ, метод энергодисперсионной рентгеновской спектроскопии и др.) позволяют существенно расширить возможности при исследовании объектов культурного наследия различного состава и размера, от миниатюр и различного рода изображений [5][6][7][8] до стеклянных и керамических предметов [9][10][11][12], а также продуктов коррозии металлических скульптур [13][14][15][16]. Кроме того, использование комплексного подхода позволяет получить информацию о структуре и составе культурных объектов, состояние которых еще в прошлом веке считалось безнадежно утраченным [17].…”

Section: Introductionunclassified

Исследование Славянского Пергамена Методами Спектроскопии Комбинационного Рассеяния Света И Люминесцентной Спектроскопии

Панькин¹,

Корогодина²,

Поволоцкая³

et al. 2021

Оптика И Спектроскопия

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In the present article the pigments palette of a parchment handwritten fragment from the collection of Finnish fragments N 29 (Library of the Russian Academy of Sciences, Finnish fragment 29, old code - 4.9.28), dating from the XIV century, was investigated. This manuscript has not been restored earlier. With the aid of Raman spectroscopy technique it was found the use of cinnabar for red shades, the mixture of indigo and gypsum pigments in various ratios for blue shades and a mixture of sulfur-arsenic pigments (orpiment and pararealgar) for yellow shades. It was performed the study of the characteristic luminescence detection capability of the pigments at the real (non-model) samples, when excited by laser radiation of various wavelengths.

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Pigment palette study of the XIX century plafond painting by Raman spectroscopy

Cited by 31 publications

References 16 publications

Characterization of a Mahamayuri Vidyarajni Sutra excavated in Lu’an, China

Characterization of a Mahamayuri Vidyarajni Sutra excavated in Lu’an, China

Investigation of Ancient Architectural Painting from the Taidong Tomb in the Western Qing Tombs, Hebei, China

Исследование Славянского Пергамена Методами Спектроскопии Комбинационного Рассеяния Света И Люминесцентной Спектроскопии

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