Photolytic Degradation as a Means of Organic Structural Determination

Juvet, Richard S.; Tanner, Roger L.; Tsao, June C. Y.

doi:10.1093/chromsci/5.1.15

Cited by 10 publications

(1 citation statement)

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“…In the latter study, a 50-µ1 cell was used and time averaging of the spectrometer output over a period of 1 day permitted use of a sample containing 0.3 µ ß of hydrogen. A new micromethod for the simultaneous determination of carbon, hydrogen, and nitrogen was developed using gas absorption chromatography with decomposition of the solutes by nickel oxide (100), and Juvet, Tanner, and Tsao (297) developed a new procedure combining mercury-sensitized photolysis with PTGC for organic structural identifications.…”

Section: Detectorsmentioning

confidence: 99%

Gas chromatography

Juvet¹,

Nogare²

1968

Anal. Chem.

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International Symposium at Rome (118, 64T), the Third International Meeting on Chromatography and Immediate Separations in Athens (467), the Fifth Eastern Germany Symposium on Gas Chromatography with authors mainly from Russian-bloc countries (149), a conference in Budapest at which the state of the art of gas chromatographic equipment was discussed along with plans for the manufacture of GC equipment in Hungary ( 7), the Analytical Chemistry Summer Symposium in Edmonton, Alberta, Canada, on "Separation Techniques" (202, 318), at which 14 of the 28 papers presented dealt with or involved gas chromatography, as well as informal symposia of the British Gas Chromatography Discussion Group (270, [384][385][386]533).

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Section: Detectorsmentioning

confidence: 99%

Gas chromatography

Juvet¹,

Nogare²

1968

Anal. Chem.

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Prelminary Reports on Structural Study via Mercury‐Sensitized Photolysis and Gas Chromatography

Tsao

1969

J Chinese Chemical Soc

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The combination of photolysis and gas-liquid -chromatography results in "fingerprints" which-are much superior 'to the pyrolysis gas chromatography method for the identification or organic compounds.With this photolysis-GLC· method. a number -of methyl ethers, benzyl ethers. isopropyl ethers and tert-butylethers were chromatographically purified and photolytically decomposed by way of mercury sensitization.The photolytic degration products were temperature programmed in a sensitive gas-liq~id chromatograph.The "fingerprint" product peaks were calculated into retention indices • .J I-values and I-values, and grouped into homologous peaks. common peaks and distinctive peaks.Identification of parent structures is obtained by the correlatton of retention indices in the above three groups of peaks.

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Neue Entwicklungen der präparativen organischen Photochemie

Adam¹

1968

Zeitschrift fuer Chemie

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Photolytic Degradation as a Means of Organic Structural Determination

Cited by 10 publications

References 0 publications

Gas chromatography

Gas chromatography

Prelminary Reports on Structural Study via Mercury‐Sensitized Photolysis and Gas Chromatography

Neue Entwicklungen der präparativen organischen Photochemie

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