Optimization of Epoxidized Methyl Acetoricinoleate Synthesis by Response Surface Methodology

Xu, Wei; Ge, Xiaodong; Cheng, De-Lin; Shao, Rong; Ding, Jianfei; Yan, Xiuhua; Liu, Tingting

doi:10.1002/ceat.201600044

Cited by 5 publications

(3 citation statements)

References 37 publications

(25 reference statements)

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“…The plot proves a high reliability of the model as the experimental yields and the predicted yields for the extraction are very close. This result is supported by other researchers [17,18]. A second-order polynomial model for the response is described by Eq.…”

Section: Resultssupporting

confidence: 85%

Empirical Model for Optimizing Shea Butter Extraction in an Unbaffled Vessel Equipped with an Impeller

Omodara¹,

Ayo²,

Emetere³

et al. 2018

ChChT

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Abstract. 1 The yield of Shea butter extracted in an unbaffled vessel equipped with an impeller was optimized by varying kneading time, kneading temperature and kneading speed using response surface method (RSM). Helical shaped impeller was mounted on a variable speed Tecmix TM 1100 kneader to knead the Shea paste. Minitab 16.1 software was used for the design and optimization of the process variables. The study indicated that the temperature and speed were highly significant on Shea butter oil yield with p-values of 0.001 and 0.002, respectively. The residual plots of the yield show that the adopted model was efficient because the experimental and the predicted yields for the extraction are very close. It was concluded that the model to be adequate.

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Section: Resultssupporting

confidence: 85%

Empirical Model for Optimizing Shea Butter Extraction in an Unbaffled Vessel Equipped with an Impeller

Omodara¹,

Ayo²,

Emetere³

et al. 2018

ChChT

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show abstract

“…On the one hand, determining the optimal operating conditions to get the highest yield of epoxidized vegetable oils has been studied by different research groups (Arumugam et al, 2014;Milchert et al, 2010;Xu et al, 2017) with the design of experiments. On the other hand, finding safe operating conditions can be obtained with similar methods.…”

Section: Introductionmentioning

confidence: 99%

Influence assessment of inlet parameters on thermal risk and productivity: Application to the epoxidation of vegetable oils

Rigaux

Buvat

Lefebvre

et al. 2021

Journal of Loss Prevention in the Process Industries

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“…A factorial design considers the potential interactions between the factors, and the conclusions are highly reproducible. Therefore, factorial design is economical in characterizing a complicated process …”

Section: Introductionmentioning

confidence: 99%

Experimental Design for Modeling and Multi‐response Optimization of Catalytic Cyclohexene Epoxidation over Polyoxometalates

Boudjema

Zerrouki

Choukchou‐Braham

2017

J Chinese Chemical Soc

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An experimental design methodology was applied to optimize cyclohexene epoxidation with hydrogen peroxide in the presence of acid‐activated montmorillonite clay supported on 11‐molybdovanado‐phosphoric acid, with the Keggin structure H4[PVMo11O40] · 13H2O (PVMo) as catalyst. The statistical study of the process was achieved through a two‐level, full‐factorial experimental design with five process parameters. The significant input variables (key factors) that influenced the performance of cyclohexene oxidation are the catalyst weight, catalyst loading, temperature, H2O2 concentration, and the reaction time. The effect of the individual parameters and their interaction effects on the cyclohexene conversion, as well as the selectivity of cyclohexane‐1,2‐diol, was determined, and a statistical model of the process was developed. The process was optimized by considering the two responses simultaneously, which allows defining the optimal regions for the significant process variables. The optimal conditions were obtained for the catalyst weight of 0.05 g, temperature of 70°C, and reaction time of 9 h, with 20% PVMo as the active phase and hydrogen peroxide as oxidant.

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Optimization of Epoxidized Methyl Acetoricinoleate Synthesis by Response Surface Methodology

Cited by 5 publications

References 37 publications

Empirical Model for Optimizing Shea Butter Extraction in an Unbaffled Vessel Equipped with an Impeller

Empirical Model for Optimizing Shea Butter Extraction in an Unbaffled Vessel Equipped with an Impeller

Influence assessment of inlet parameters on thermal risk and productivity: Application to the epoxidation of vegetable oils

Experimental Design for Modeling and Multi‐response Optimization of Catalytic Cyclohexene Epoxidation over Polyoxometalates

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