“…Then, the deprotonation of glucose in an alkaline medium triggers isomerization to an enediol form, which in contact with Cu(III) gets oxidized to gluconolactone and then further hydrolyzes to gluconic acid. [31][32][33][34] Based on the electrocatalytic activity of Cu 4 V 2.15 O 9.38 superstructures towards oxidation of glucose, the modied GC electrode was evaluated as a glucose sensor. Fig.…”