The initial carbon condensate containing nickel-iron nanoparticles with a graphite conversion was synthesized in the high-frequency carbon-helium arc plasma at ambient pressure. The nickel-iron particles were extracted by the treatment of the carbon condensate with nitric and hydrochloric acids. Undissolved residue and dissolved sample were received. Undissolved residue has both the structure and magnetic properties of (MR/Ms = 0.30, Hc = 270 Oe). Lack of hysteresis loops for the dissolved sample shown that metals are in the paramagnetic state.