NH<sub>4</sub>I-promoted electrosynthesis of 2-aminothiazole derivatives from ketone compounds and NH<sub>4</sub>SCN

Zhang, Chaowei; Yuan, Gaoqing

doi:10.1039/d3cc03547f

Chem. Commun.

2023

DOI: 10.1039/d3cc03547f

|View full text |Cite

NH₄I-promoted electrosynthesis of 2-aminothiazole derivatives from ketone compounds and NH₄SCN

Chaowei Zhang,

Gaoqing Yuan

Abstract: A novel and efficient electrochemical synthesis of 2-aminothiazole derivatives from ketones and NH4SCN is described. Under the co-action of NH3 and iodine free radicals or iodine (I2) electrochemically generated in...

Help me understand this report

Search citation statements

Order By: Relevance

Paper Sections

Select...

Citation Types

Supporting

Mentioning

Contrasting

Year Published

2024

Publication Types

Select...

Article2

Relationship

Self Cite1

Independent1

Authors

Journals

Cited by 2 publications

References 19 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

Telescoping Synthesis of 4‐Organyl‐5‐(organylselanyl)thiazol‐2‐amines Promoted by Ultrasound

Hellwig,

Bartz,

Santos

et al. 2024

ChemPlusChem

View full text Add to dashboard Cite

In this work, we describe the synthesis of new 4‐organyl‐5‐(organylselanyl)thiazol‐2‐amine hybrids through a one‐pot two‐step protocol. The transition metal‐free method involves the use of ultrasound as an alternative energy source and Oxone® as oxidant. To obtain the products, a telescoping approach was used, in which 4‐organylthiazol‐2‐amines were firstly prepared under ultrasonic irradiation, followed by the addition of diorganyl diselenides and Oxone®. Thus, 16 compounds were prepared, with yields ranging from 61 % to 98 %, using 2‐bromoacetophenone derivatives and diorganyl diselenides as easily available starting materials.

show abstract

Telescoping Synthesis of 4‐Organyl‐5‐(organylselanyl)thiazol‐2‐amines Promoted by Ultrasound

Hellwig,

Bartz,

Santos

et al. 2024

ChemPlusChem

View full text Add to dashboard Cite

show abstract

A Facile Electrosynthesis of Polysubstituted Oxazoles from Aromatic Ketones and Benzylamines under Mild Conditions

Xiao,

Yuan

2024

ChemistrySelect

Self Cite

View full text Add to dashboard Cite

show abstract

scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.

Contact Info

customersupport@researchsolutions.com

10624 S. Eastern Ave., Ste. A-614

Henderson, NV 89052, USA

Blog Terms and Conditions API Terms Privacy Policy Contact Cookie Preferences Do Not Sell or Share My Personal Information

Made with 💙 for researchers

Part of the Research Solutions Family.

NH₄I-promoted electrosynthesis of 2-aminothiazole derivatives from ketone compounds and NH₄SCN

Abstract: A novel and efficient electrochemical synthesis of 2-aminothiazole derivatives from ketones and NH4SCN is described. Under the co-action of NH3 and iodine free radicals or iodine (I2) electrochemically generated in...

Cited by 2 publications

References 19 publications

Telescoping Synthesis of 4‐Organyl‐5‐(organylselanyl)thiazol‐2‐amines Promoted by Ultrasound

Telescoping Synthesis of 4‐Organyl‐5‐(organylselanyl)thiazol‐2‐amines Promoted by Ultrasound

A Facile Electrosynthesis of Polysubstituted Oxazoles from Aromatic Ketones and Benzylamines under Mild Conditions

Contact Info

Product

Resources

About

NH4I-promoted electrosynthesis of 2-aminothiazole derivatives from ketone compounds and NH4SCN

Abstract: A novel and efficient electrochemical synthesis of 2-aminothiazole derivatives from ketones and NH4SCN is described. Under the co-action of NH3 and iodine free radicals or iodine (I2) electrochemically generated in...

Cited by 2 publications

References 19 publications

Telescoping Synthesis of 4‐Organyl‐5‐(organylselanyl)thiazol‐2‐amines Promoted by Ultrasound

Telescoping Synthesis of 4‐Organyl‐5‐(organylselanyl)thiazol‐2‐amines Promoted by Ultrasound

A Facile Electrosynthesis of Polysubstituted Oxazoles from Aromatic Ketones and Benzylamines under Mild Conditions

Contact Info

Product

Resources

About

NH₄I-promoted electrosynthesis of 2-aminothiazole derivatives from ketone compounds and NH₄SCN