Multi-analyte gas chromatography-mass spectrometry method to monitor bisphenols, musk fragrances, ultraviolet filters, and pesticide residues in seafood

Petrarca, Mateus Henrique; Fernandes, José O.; Marmelo, Isa; Marques, António; Cunha, Sara C.

doi:10.1016/j.chroma.2021.462755

Cited by 24 publications

(10 citation statements)

References 37 publications

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“…The method verified using mackerel fillet by Wongmaneepratip, Leong and Yanga [ 40 ] for pyrethroids achieved standard deviations (SD) of 4.91 to 13.69%. The majority of agrochemicals analyzed by Petrarca et al [ 41 ] and Kaczyński et al [ 42 ] achieved a repeatability RSD ≤ 20% in the analysis of agrochemicals in seafood.…”

Section: Resultsmentioning

confidence: 99%

“…The mean concentration of organochlorine recoveries in spiked fish samples was 91% with RSD < 20% in the Cho, Lee and Jung [ 44 ] study. The majority of agrochemicals presented mean recoveries within the range of 70–120% and repeatability RSD ≤ 20% in bivalves, lean and fatty fishes [ 41 ]. The method proposed by Wongmaneepratip, Leong and Yanga [ 40 ] applied to pyrethroid analysis in salmon, seabass, threadfin fish, tiger prawn, vannamei prawn, shrimp, squid, grand jackknife clam, and oyster provided recoveries of 75.95–96.81%.…”

Section: Resultsmentioning

confidence: 99%

“…Wongmaneepratip, Leong and Yanga [ 40 ] achieved LOQs of 0.54–0.85 ng g −1 for pyrethroids in seafood. The method’s detection limits ranged from 0.05 to 1.2 μg kg −1 in the Petrarca et al [ 41 ] study.…”

Section: Resultsmentioning

confidence: 99%

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Agrochemical Residues in Fish and Bivalves from Sepetiba Bay and Parnaiba River Delta, Brazil

Miranda

Fogaça

Cunha

et al. 2022

IJERPH

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Accumulation of pesticides has a harmful impact on the environment and human health. The main goal of this work was to develop a method to determine and quantify the residues of thirteen pesticides in edible fish and bivalves such as parati (Mugil curema), seabass (Centropomus ssp.), mullet (Mugil brasiliensis), clams (Anomalocardia brasiliana) and mussel (Mytilus galloprovincialis) collected from Sepetiba Bay and Parnaiba River Delta (Brazil) between 2019 and 2020. Matrix solid-phase dispersion (MSPD) was used for extraction and quantification through gas chromatography coupled to tandem mass spectrometry (GC-MS/MS). The method was validated (linearity, accuracy and precision) for fatty fish (Salmo salar), lean fish (Mugil curema) and bivalves (Mytilus edulis). The survey found linear correlation coefficients (r) equal to or greater than 0.9 for almost all analytes. The relative standard deviations (RSD) of five replicates were less than 20% for almost all analytes at different concentrations in lean fish, fatty fish and bivalves. Most analytes showed satisfactory accuracy. Alachlor herbicide was found in samples of seabass, mussels, clams and parati with levels ranging between 0.55 to 420.39 μg kg−1 dw. Ethion was found in parati (maximum 211.22 μg kg−1 dw), mussels (15.1 μg kg−1 dw) and clams (maximum 44.50 μg kg−1 dw). Alachlor was found in clams (maximum 93.1 μg kg−1 dw), and bifenthrin was found in parati (maximum 43.4 μg kg−1 dw) and clams (maximum 42.21 μg kg−1 dw). The validated method was satisfactory for the determination of eleven pesticides in the fatty fish matrix, and thirteen pesticides in the samples of lean fish and bivalves. The presence of alachlor, ethion and bifenthrin stands out.

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Section: Resultsmentioning

confidence: 99%

Section: Resultsmentioning

confidence: 99%

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Agrochemical Residues in Fish and Bivalves from Sepetiba Bay and Parnaiba River Delta, Brazil

Miranda

Fogaça

Cunha

et al. 2022

IJERPH

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“…Sample extraction was performed as described in Petrarca et al [ 37 ]. Briefly, homogenized fish (≈1 g) or NBIO fractions (≈250 mg) were weighed into amber-glass vials, and internal standards were added.…”

Section: Methodsmentioning

confidence: 99%

“…ChemStation software was used for data processing. Chromatographic and detection specifications were reported elsewhere [ 37 ].…”

Section: Methodsmentioning

confidence: 99%

Effects of Green Tea Marinade in the Bioaccessibility of Tonalide and Benzophenone 3 in Cooked European Seabass

et al. 2022

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Fish consumption is an indicator of human exposure to personal care products (PCP) such as tonalide (AHTN) and benzophenone 3 (BP3). Although most fish consumed is cooked, the impact of cooking procedures on PCP levels is difficult to evaluate. Hence, the aim of this work was to provide thorough information on the stability and bioaccessibility of AHTN and BP3 upon cooking and in vitro digestion. A green tea (Camellia sinensis) marinade, rich in polyphenol, was used as mitigating strategy to reduce these contaminants. Roasting and frying reduced AHTN and BP3 levels in European seabass (Dicentrarchus labrax) spiked samples. Additionally, the green tea marinade promoted a reduction of up to 47% AHTN and 35% BP3. Bioaccessibility of AHTN was higher (up to 45%), and increased with the use of green tea marinades. BP3 showed a bioaccessibility below 19% in all cooked samples. Overall, a decrease in PCP levels was observed after cooking; this decrease was even more pronounced when marination was previously used. However, this decrease is cancelled out by the fact that the bioaccessible fraction of the contaminants increases in an inverse way; therefore, none of these processes can be considered a mitigating alternative.

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Occurrence of Fragrances in the Marine Environment

Guerra-Martín,

Lodoso-Ruiz,

Trujillo-Rodríguez

et al. 2023

The Handbook of Environmental Chemistry

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Multi-analyte gas chromatography-mass spectrometry method to monitor bisphenols, musk fragrances, ultraviolet filters, and pesticide residues in seafood

Cited by 24 publications

References 37 publications

Agrochemical Residues in Fish and Bivalves from Sepetiba Bay and Parnaiba River Delta, Brazil

Agrochemical Residues in Fish and Bivalves from Sepetiba Bay and Parnaiba River Delta, Brazil

Effects of Green Tea Marinade in the Bioaccessibility of Tonalide and Benzophenone 3 in Cooked European Seabass

Occurrence of Fragrances in the Marine Environment

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