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SPONSORING/MONITORING AGENCY REPORT NUMBER(S)AFRL-RX-WP-TP-2012-0390
DISTRIBUTION/AVAILABILITY STATEMENTApproved for public release; distribution unlimited. Preprint to be submitted to Metallurgical and Materials Transactions.
SUPPLEMENTARY NOTESThe U.S. Government is joint author of this work and has the right to use, modify, reproduce, release, perform, display, or disclose the work. PA Case Number and clearance date: 88ABW-2012-2970, 21 May 2012. This document contains color.
ABSTRACTRene88 samples were investigated using atom probe tomography and x-ray diffraction using a monochromated synchrotron beam with different energy values to determine the preferred site occupancy of various alloying elements within the ordered γ' precipitates. Samples were solutionized and cooled at 24 degree C/min with subsequent aging at 760 degrees C. The synchrotron-based x-ray diffraction results indicate that niobium prefers to reside on the aluminum sublattice site of the γ' phase. Additionally, the experimental results also indicate that chromium prefers the nickel sublattice sites while cobalt is likely to occupy both the aluminum and nickel sublattice sites. The x-ray results on the chromium occupancy disagree with atom probe results from the same alloy that indicate that chromium prefers the aluminum sublattice sites. Modeling studies indicate cobalt has no strong site preference.
SUBJECT TERMS
AbstractRene88 samples were investigated using atom probe tomography and x-ray diffraction using a monochromated synchrotron beam with different energy values to determine the preferred site occupancy of various alloying elements within the ordered γ' precipitates. Samples were solutionized and cooled at 24 degree C/min with subsequent aging at 760 degrees C. The synchrotron-based x-ray diffraction results indicate that niobium prefers to reside on the aluminum sublattice site of the γ' phase. Additionally, the experimental results also indicate that chromium prefers the nickel sublattice sites while cobalt is likely to occupy both the aluminum and nickel sublattice sites. The x-ray results on the chromium occupancy disagree with atom probe results from the same alloy that indicate that chromium prefers the aluminum sublattice sites. Modeling studies indicate cobalt has no strong site preference.