Abstract:Microscopic, and X‐ray examinations of a series of steatite compositions reveal that the body having the best dielectric properties Also has the simplest and most homogeneous physical structure. It is believed that the attainment of similar physical structures in other ceramic bodies will lead to improvements in dielectric properties.
This empirical finding is in accordance with present theories of conduction in crystals. It depends on the contribution to conductivity and dielectric loss made by imperfections … Show more
“…Microhardness testing in metal lurgy (30, ISO), a new microindenter for use with a metallurgical microscope (43), and a simple and accurate microhardness testing device (24) are applications in the metallurgical field. Among technical applications may be mentioned the microscopical and x-ray examination of some steatite bodies (115), and the microscopy of high temperature phenomenon in ceramics (19).…”
Section: Miscellaneous Methods and Applicationsmentioning
confidence: 99%
“…Applied Phys., 18, 522-9 (1947). (115) Mateosian, E. der, Iron Age, 159, 51-3 (1947). (116) Matolsky, A. G., Nature, 161, 353 (1948).…”
“…Microhardness testing in metal lurgy (30, ISO), a new microindenter for use with a metallurgical microscope (43), and a simple and accurate microhardness testing device (24) are applications in the metallurgical field. Among technical applications may be mentioned the microscopical and x-ray examination of some steatite bodies (115), and the microscopy of high temperature phenomenon in ceramics (19).…”
Section: Miscellaneous Methods and Applicationsmentioning
confidence: 99%
“…Applied Phys., 18, 522-9 (1947). (115) Mateosian, E. der, Iron Age, 159, 51-3 (1947). (116) Matolsky, A. G., Nature, 161, 353 (1948).…”
“…protoenstatite) and 30 % of glassy phase [15]. The development of microstructure and sintering behavior of steatite thereby depend on the ratio of formed crystalline and liquid phases [16][17][18]. The steatite's dielectric properties are strongly dependent on the temperature range and/or cycling (i.e.…”
Section: Introductionmentioning
confidence: 99%
“…Even though steatite is a valuable dielectric material, very few studies researched its sintering related properties [14][15][16][17][18][19][20]. This investigation provides insight into sintering behavior of steatites based of natural raw materials, i.e.…”
The influence of the sintering method on the mineral phase transformations and development of the crystalline microstructure of steatite ceramics was investigated. The steatite samples were fabricated from talc and bentonite as low-cost raw materials. Feldspar and barium carbonate, as fluxing agents, were altered in the steatite composition. Dilatometric analysis was applied in the monitoring of the dimensional changes and thereby densification of steatite during the traditional sintering (TS) procedure up to 1200 °C. Spark plasma sintering (SPS) method was used under the following sintering conditions: 100 °C/min heating rate, uniaxial pressure of 50 MPa; sintering temperature 800 °C/1 min or 1000 °C/2 min. Crystallinity changes and mineral phase transition during sintering were observed by X-ray diffraction technique. Microstructural visualization of the samples and the spatial arrangements of individual chemical elements were achieved via scanning electron microscopy equipped with the EDS mapping. It was found that SPS sintering facilitated all microstructural changes during high temperature treatment and shifted them to lower temperatures. SPS treatment conducted at 1000 °C resulted in maximum densification of the steatite powder compacts and the formation stabilized protoenstatite structure.
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