2016
DOI: 10.4028/www.scientific.net/msf.846.479
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Mechanochemical Synthesis of CNT/ZnO Hybrid Materials

Abstract: A study on the synthesis of multiwalled carbon nanotubes (MWCNT) and zinc oxide (ZnO) hybrid materials using the mecahnochemical technique has been conducted. MWCNT was dispersed in sodium dodecyl sulfate (SDS) solution. ZnO was formed at milling time between 2 and 5 hours, where at 10 hours the XRD results showed only small peaks of ZnO. This suggests that at longer milling time, the ZnO crystals were either become amorphous or have reduced in sized so as not to be detected using XRD. ZnO has also been doped … Show more

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Cited by 2 publications
(2 citation statements)
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“…The acid treatment debundles the nanotubes and disposes functional groups on their sidewalls which serve as anchorage points for the ZnO nanoparticles. Aziz et al have dispersed CNT in sodium dodecyl sulphate followed by ball milling the ZnO that was previously obtained by hydrothermal synthesis [76]. CNT have also been grown by spray pyrolysis methods and purified thereafter to get rid of the iron impurities; they were then sintered at 700 ∘ C with ZnO prepared by oxidizing Zn dust at very high temperatures under oxygen rich conditions [77].…”
Section: Cnt-zno Synthesis Carbon Nanotubes and Zno Nanocomposites Hmentioning
confidence: 99%
“…The acid treatment debundles the nanotubes and disposes functional groups on their sidewalls which serve as anchorage points for the ZnO nanoparticles. Aziz et al have dispersed CNT in sodium dodecyl sulphate followed by ball milling the ZnO that was previously obtained by hydrothermal synthesis [76]. CNT have also been grown by spray pyrolysis methods and purified thereafter to get rid of the iron impurities; they were then sintered at 700 ∘ C with ZnO prepared by oxidizing Zn dust at very high temperatures under oxygen rich conditions [77].…”
Section: Cnt-zno Synthesis Carbon Nanotubes and Zno Nanocomposites Hmentioning
confidence: 99%
“…To synthesize ZnO NPs by this method, anhydrous ZnCl 2 and Na 2 CO 3 are used as starting materials and NaCl as a reaction medium and separator of ZnO NPs [4,40]. Several composites such as fluorapatite-zinc oxide (FAp-ZnO) composite nanopowder [41], Mn-doped ZnO nanoparticles [42], silver doped ZnO NPs [43], and carbon nanotubes (CNT)/ ZnO hybrid materials [44] have been synthesized by the mechanochemical process. Micron-and submicron-sized emulsions synthesis methods are usually referred to as microemulsions.…”
Section: Chemical Methodsmentioning
confidence: 99%