“…The temperatures of the ion trap, manifold, and transfer line were 150 °C, 40 °C, and 180 °C, respectively. The MS detector monitored ions from 72 to 79, 89 to 93, 101 to 107, and 119 to 121 (m/z) (Correa et al, 2012 ; Corrêa and Arbilla, 2007 , 2006 ; Daemme, 2016a ; Daemme, 2016b ; Garcia et al, 2013 ; Macedo et al, 2017 ; Martins et al, 2016 , 2007 ). The calibration was performed with a standard BTEX solution (Supelco EPA TO-1 Mix 1A) by external standardisation with concentrations of 0.10, 0.20, 0.50, 1.00, 2.00, and 4.00 ng mL −1 , as an acceptance criterion of the analytical curve determination coefficients higher than 0.99.…”