“…As a novel sample pretreatment technique, DLLME coupling with gas chromatography (GC) or high performance liquid chromatography (HPLC) for the determination of organic compounds in environmental water samples has received greate concerns [15,[17][18][19][20][21][22]. For the studies, BTEX, polycyclic aromatic hydrocarbons (PAHs), organophosphorous pesticides (OPPs), organochlorine pesticides (OCPs), organosulphur pesticides (OSPs), nitromatic compounds, polychlorinated biphenyls (PCBs), triazine herbicides, phthalate esters (PAEs), decabrominated diphenyl ether, aromatic amines, phenoxyacetic acid herbicides, bisphenol A, and endocrine-disrupting phenols, for examples, are depicted [15, in Table 1.…”