Is it still possible, necessary and beneficial to perform research in ICP-atomic emission spectrometry?

Mermet, Jean‐Michel

doi:10.1039/b416511j

Cited by 93 publications

(61 citation statements)

References 15 publications

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“…ICP-OES is still a most appropriate technique for elemental analysis [12], especially for those light elements, which are very important for advanced ceramics [7]. It is also noticeable that slurry introduction technique for analytical atomic spectrometry has been used for the analysis of many advanced materials, but details of various slurry preparation and characterization are still very scarce [13].…”

Section: Introductionmentioning

confidence: 99%

Direct determination of impurities in high purity silicon carbide by inductively coupled plasma optical emission spectrometry using slurry nebulization technique

Zheng

Qiu

Zhang

et al. 2006

Analytica Chimica Acta

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A novel method for the determination of Al, Ca, Cr, Cu, Fe, Mg, Mn, Ni and Ti in high purity silicon carbide (SiC) using slurry introduction axial viewed inductively coupled plasma optical emission spectrometry (ICP-OES) was described. The various sizes of SiC slurry were dispersed by adding dispersant polyethylene imine (PEI). The stability of slurry was characterized by zeta potential measurement, SEM observation and signal stability testing. The optimal concentration of PEI was found to be 0.5 wt% for the SiC slurry. Analytical results of sub-m size SiC by the slurry introduction were in good accordance with those by the alkaline fusion method which verified that determination could be calibrated by aqueous standards. For m size SiC, results of most elements have a negative deviation and should be calibrated by the Certified Reference Material slurry. Owing to a rather low contamination in the sample preparation and stability of the slurry, the limits of detection (LODs), which are in the range of 40-2000 ng g −1 , superior to those of the conventional nebulization technique by ICP-OES or ICP-MS.

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Section: Introductionmentioning

confidence: 99%

Direct determination of impurities in high purity silicon carbide by inductively coupled plasma optical emission spectrometry using slurry nebulization technique

Zheng

Qiu

Zhang

et al. 2006

Analytica Chimica Acta

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“…Otherwise, the accuracy of analysis can be notably affected. 10 Accuracy is one of the principal performance parameters to be evaluated during the implementation of an analytical procedure and it is an essential requirement for the quality control of measurements in environmental chemistry.…”

Section: Introductionmentioning

confidence: 99%

Comparison of USEPA 3050B and ISO 14869-1: 2001 digestion methods for sediment analysis by using FAAS and ICP-OES quantification techniques

Navarro¹,

Tagle²,

Larrea³

et al. 2011

Quím. Nova

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Recebido em 19/7/10; aceito em 25/2/11; publicado na web em 5/5/11 A study of the partial USEPA 3050B and total ISO 14869-1:2001 digestion methods of sediments was performed. USEPA 3050B was recommended as the simpler method with less operational risk. However, the extraction ability of the method should be taken in account for the best environmental interpretation of the results. FAAS was used to quantify metal concentrations in sediment solutions. The alternative use of ICP-OES quantification should be conditioned by a previous detailed investigation and eventual correction of the matrix effect. For the first time, the EID method was employed for the detection and correction of the matrix effect in sediment ICP-OES analysis. Finally, some considerations were made about the level of metal contamination in the area under study.

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“…The ICP-OES method has become a routine analytical technique for metal determination; however, the information related to method validation are scarce, and research on this field is still needed (Mermet 2005). Several studies present the use of ICP-OES for metals determination in tea or other food samples (Mitic et al 2012;Froes et al 2014).…”

Section: Introductionmentioning

confidence: 99%

Validation and measurement uncertainty evaluation of the ICP-OES method for the multi-elemental determination of essential and nonessential elements from medicinal plants and their aqueous extracts

et al. 2014

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Background: The paper presents the development, validation, and evaluation of measurement uncertainty of a method for quantitative determination of essential and nonessential elements in medicinal plants and their aqueous extracts by using inductively coupled plasma optical emission spectrometry. Methods: The detailed validation of the analytical procedure and calculation of the measurement uncertainty budget allowed the recognition of the methods' critical points.

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Is it still possible, necessary and beneficial to perform research in ICP-atomic emission spectrometry?

Cited by 93 publications

References 15 publications

Direct determination of impurities in high purity silicon carbide by inductively coupled plasma optical emission spectrometry using slurry nebulization technique

Direct determination of impurities in high purity silicon carbide by inductively coupled plasma optical emission spectrometry using slurry nebulization technique

Comparison of USEPA 3050B and ISO 14869-1: 2001 digestion methods for sediment analysis by using FAAS and ICP-OES quantification techniques

Validation and measurement uncertainty evaluation of the ICP-OES method for the multi-elemental determination of essential and nonessential elements from medicinal plants and their aqueous extracts

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