“…1H, N ax ), 3.14 -3.01 (m, 2H, N eq + γ ax ), 2.92 (s, 3H, AMe), 2.67 -2.57 (m, 1H, α), 2.53 -2.43 (m, 1H, γ eq ), 2.17 -2.07 (m, 1H, α), 2.06 -1.97 (m, 1H, β), 1.96 -1.87 (m, 1H, β), 1.62 (s, 3H, BMe), 1.58 (s, 3H, MeS-). 13 Table 3 for the details). Then, 600 µL of the stock solution were transferred, under N 2 , into a NMR tube.…”