2008
DOI: 10.1007/s12274-008-8008-5
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In situ TEM measurements of the mechanical properties and behavior of WS2 nanotubes

Abstract: The mechanical properties of individual WS 2 nanotubes were investigated and directly related to their atomic structure details by in situ transmission electron microscope measurements. A brittle mode deformation was observed in bending tests of short (ca. 1 μm in length) multilayer nanotubes. This mode can be related to the atomic structure of their shells. In addition, longer nanotubes (6 7μm in length) were deformed in situ scanning electron microscope, but no plastic deformation was detected. A "sword-in-s… Show more

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Cited by 57 publications
(43 citation statements)
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“…Regarding the snapshots of deformed shapes in Fig. 11, a kind of flattening of the cross-section of the nanotube can be qualitatively seen, as has been reported (Yakobson et al, 1996;Iijima et al, 1996;Wang et al, 2008). This resembles the so-called Brazier effect (Brazier, 1927) in continuum mechanics.…”
Section: Tablesupporting
confidence: 71%
“…Regarding the snapshots of deformed shapes in Fig. 11, a kind of flattening of the cross-section of the nanotube can be qualitatively seen, as has been reported (Yakobson et al, 1996;Iijima et al, 1996;Wang et al, 2008). This resembles the so-called Brazier effect (Brazier, 1927) in continuum mechanics.…”
Section: Tablesupporting
confidence: 71%
“…These generally lack real time structural monitoring, and do not permit a one-to-one correlation between mechanical data and internal structural evolution. Recently, in situ mechanical characterization of individual nanowires with diameters from tens to hundreds of nanometers inside a TEM were realized under various loading geometries, such as bending [8], buckling [9], and compression [3]. However, use of the most efficient and easy-to-interpret tensile testing method for measuring intrinsic mechanical properties of exceedingly small nanowire samples inside a TEM poses significant challenges due to difficulties associated with sample clamping, alignment and accurate measurements of load and displacement.…”
Section: Introductionmentioning
confidence: 99%
“…Recently, in-situ characterization techniques [122][123][124][125][126][127] have turned out to be very useful for mechanical testing of NWs. However, due to lack of standardization and several complexities, there is large variance in the reported values, and the elastic properties for these NWs were found to be very different from their bulk counterparts.…”
Section: E Mechanical Propertiesmentioning
confidence: 99%