2021
DOI: 10.3390/inorganics9110085
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In Situ and In Operando Techniques to Study Li-Ion and Solid-State Batteries: Micro to Atomic Level

Abstract: This work summarizes the most commonly used in situ techniques for the study of Li-ion batteries from the micro to the atomic level. In situ analysis has attracted a great deal of interest owing to its ability to provide a wide range of information about the cycling behavior of batteries from the beginning until the end of cycling. The in situ techniques that are covered are: X-ray diffraction (XRD), Raman spectroscopy, X-ray photoelectron spectroscopy (XPS), Scanning Electron Microscopy (SEM), Transmission El… Show more

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Cited by 7 publications
(2 citation statements)
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“…• Crystallographic analysis using electron backscatter diffraction. • Minimal sample manipulation [207].…”
Section: X-ray Computed Tomographymentioning
confidence: 99%
“…• Crystallographic analysis using electron backscatter diffraction. • Minimal sample manipulation [207].…”
Section: X-ray Computed Tomographymentioning
confidence: 99%
“…Currently, common detection methods for lithium-ion batteries include disassembly characterization methods and in-situ characterization methods. Disassembly methods, such as scanning electron microscopy (SEM) 7 , 8 , provide rich information about battery material properties. However, they may alter the internal structure during disassembly, leading to less accurate information.…”
Section: Introductionmentioning
confidence: 99%