“…Undoubtedly, a few peaks representing the crystalline phases of hematite (␣-Fe 2 O 3 ) or maghemite (␥-Fe 2 O 3 ) and magnetite (Fe 3 O 4 ) in the range of 2Â = 30-60 • are visible in the XRD pattern of M2 and more prominently in M3. The reflection peaks (in relevance to the JCPDS card numbers 19-629 and 39-1346) observed for M3, are in close agreement with the corresponding peak intensities for magnetite, e.g., (2 2 0), (3 1 1), (4 0 0), (4 2 2) and (5 1 1), reported for iron oxides by other researchers [50][51][52]. As reported by Lee et al [52], due to the very small size and amount of iron oxide nanoparticles, sometime their phase assignment is ambiguous.…”