2007
DOI: 10.1088/0960-1317/17/11/020
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High resolution deformation and damage detection using fluorescent dyes

Abstract: We demonstrate the application of fluorescence microscopy to detect nanoscale deformation and damage in polymeric materials. Fluorescent probes were dispersed in a poly-dimethyl siloxane matrix, and were subsequently strained with and without the presence of edge cracks. This technique can reveal cracks that are invisible to white light microscopy (smaller than 250 nm), and is outperformed only by high resolution electron or scanning probe microscopy. The technique may find applications in early stage damage d… Show more

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Cited by 10 publications
(7 citation statements)
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“…The molecular fluorescent probes are originally used in molecular biology, the pre -dispersed probes in the matrix are subjected to changes in the fluorescent intensity as a result of any topological changes in the matrix, it has been suggested that it can detect nanoscale cracks in polymers [158]. The major limitations of this technique are that it requires a uniform pre dispersion of the die and transparent polymer specimen in addition to geometry limitation of the specimen due to use of the fluorescent microscope.…”
Section: Microcracking Due To Hygrothermal Ageingmentioning
confidence: 99%
See 1 more Smart Citation
“…The molecular fluorescent probes are originally used in molecular biology, the pre -dispersed probes in the matrix are subjected to changes in the fluorescent intensity as a result of any topological changes in the matrix, it has been suggested that it can detect nanoscale cracks in polymers [158]. The major limitations of this technique are that it requires a uniform pre dispersion of the die and transparent polymer specimen in addition to geometry limitation of the specimen due to use of the fluorescent microscope.…”
Section: Microcracking Due To Hygrothermal Ageingmentioning
confidence: 99%
“…Furthermore, the signal measuring techniques require a highly trained operator to acquire and interpret the data, the signals are also corrupted by the structural and electrical noise in addition to attenuation and scattering.The uses of high resolution inspection techniques such as electron microscopy and electron probing are suitable only for certain specimen type and size and they are in general expensive to use. Another class of cracks monitoring techniques are based on employing fiber optic probe or fluorescent probe[4,151,158].…”
mentioning
confidence: 99%
“…For such experimental systems, information from multiple optical indicators can be mathematically combined to further reduce the uncertainty of a position measurement and to enable an orientation measurement with low uncertainty. Related measurements have diverse applications in microtechnology, nanotechnology, biology, materials and metrology (Freeman, 2001;Ropp et al, 2013;Berfield et al, 2006Berfield et al, , 2007McGray et al, 2013;Samuel et al, 2007;Yoshida et al, 2011;Teyssieux et al, 2011;Ueno et al, 2010). Recently, constellations of fluorescent nanoparticles indicating the motion of microscopic actuators were localized and tracked, demonstrating the utility of the measurement method (McGray et al, 2013;Copeland et al, 2015).…”
Section: Introductionmentioning
confidence: 99%
“…Resembling these biological systems, optical mechanotransducers emerge as valuable engineered materials capable of converting mechanical events, either tension or pressure, into readable and processable optical outputs. Indeed, smart materials that tune their optical properties upon deformation or compression are of great interest within actual technology since they allow easy access to unique applications, from damage sensing to security inks to rewritable paper …”
Section: Introductionmentioning
confidence: 99%
“…
Indeed, smart materials that tune their optical properties upon deformation or compression are of great interest within actual technology since they allow easy access to unique applications, from damage sensing [2][3][4][5] to security inks [ 6,7 ] to rewritable paper. [ 8 ] Switching the material luminescence between two different emitting states, with either distinct color or intensity, by altering mechanically-shearing, grinding or rubbing-the microenvironment of fl uorophores within solid materials can serve as a general protocol for optical mechanotransduction.
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mentioning
confidence: 99%