2017
DOI: 10.1007/s00604-017-2498-3
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Hierarchical C-N doped NiO with dual-head echinop flowers for ultrasensitive monitoring of epinephrine in human blood serum

Abstract: E m r a n , M o h a m m e d Y., Kh alifa, H e s h a m , Go m a a , H a s s a ni e n, S h e n a s h e n , M o h a m e d A., Akh t ar, N a e e m , M e k a wy, M o a t a z, F a h e e m , Ah m e d a n d El-S af ty, S h e rif (2 0 1 7) Hi e r a r c hic al C-N d o p e d Ni O wit h d u al-h e a d e c hi n o p flo w e r s fo r ul t r a s e n si tiv e m o ni t o ri n g of e pi n e p h ri n e in h u m a n bloo d s e r u m . Mi c r o c hi mic a Act a, 1 8 4 (1 1). p p. 4 5 5 3-4 5 6 2. IS S N 0 0 2 6-3 6 7 2 Do w nlo a d… Show more

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Cited by 82 publications
(48 citation statements)
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References 36 publications
(40 reference statements)
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“…The electrochemical activity of the NMCS/GCE was investigated using cyclic voltammetry (CV) in 10 mL of 0.1 m KCl containing 1 × 10 −3 m [Fe(CN) 6 ] 3− in the potential range of −0.2 to 0.7 V (vs Ag/AgCl), and at a scan rate of 100 mV s −1 . The [Fe(CN) 6 ] 3− was used as a redox probe to check the key factors affecting the charge transfer along the designated electrode surfaces including charge transfer properties, electrocatalytic activity, and surface chemistry (Figure S2A, Supporting Information) . Results show that the efficient electron transfer activity of the NMCS/GCE is higher than that of bare GCE.…”
Section: Resultsmentioning
confidence: 99%
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“…The electrochemical activity of the NMCS/GCE was investigated using cyclic voltammetry (CV) in 10 mL of 0.1 m KCl containing 1 × 10 −3 m [Fe(CN) 6 ] 3− in the potential range of −0.2 to 0.7 V (vs Ag/AgCl), and at a scan rate of 100 mV s −1 . The [Fe(CN) 6 ] 3− was used as a redox probe to check the key factors affecting the charge transfer along the designated electrode surfaces including charge transfer properties, electrocatalytic activity, and surface chemistry (Figure S2A, Supporting Information) . Results show that the efficient electron transfer activity of the NMCS/GCE is higher than that of bare GCE.…”
Section: Resultsmentioning
confidence: 99%
“…Several analytical techniques have been used for DA detection, such as chromatography, fluorimetry, rapid liquid chromatography/tandem mass spectrometry (LC‐MS/MS), chemiluminescence, and plasmonic probing . Although these techniques show high sensitivity and selectivity toward DA, but they associated with complex and time‐consuming protocol, specific procedures, and expensive tools for biosensing preparations . Thus, the development of simple and inexpensive analytical methods for selective and sensitive detection of DA is of particular interest.…”
Section: Introductionmentioning
confidence: 99%
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“…4e and S16. The equivalent circuit comprises an electrolyte resistance (Ohmic resistance R s , which refers to the intercept impedance on the real axis and corresponds to solution resistance), charge transfer resistance (R ct , which results from the electrochemical interaction at the electrode/electrolyte interface and particle/particle contact), constant phase element, and Warburg impedance of the Li + ion diffusion into the electrode (W f ; which is related to the low-frequency region of the straight line) [25,[44][45][46][47]. The semicircular arc at the highest frequency range is relative to the R ct value, which is approximately equal to the numerical value of the diameter of the semicircle on the Z real axis.…”
Section: Half-cell Design Based On Power Hierarchy Vst-(i-vii)@c Cathmentioning
confidence: 99%
“…Accordingly, these materials are widely applied in many important fields. Among them, nickel oxide (NiO) is an important semiconductor functional material [2], which is widely used in lithium ion batteries [3], electrocatalysis [4], thermal catalysis [5], gas sensor [6], electrochemistry [7,8], optical sensor [9] and biosensors [10][11][12][13][14] fields. Therefore, the preparation of various mesoporous NiO nanomaterials has become a research hotspot.…”
Section: Introductionmentioning
confidence: 99%