“…The root of the volume fraction determined by 3DAP analysis is proportional to the transition temperature shift and the increase in hardness or yield strength. This relationship is widely found in surveillance data [59,69,71], MTR irradiation data [77,79] and also various changed particle irradiation data [37], and is irrespective of the Cu content and irradiation conditions. Figure 8 shows an example of the linear relationship between the cluster volume fraction and transition temperature shift [59].…”
Section: Characteristics Of Solute Clusterssupporting
confidence: 53%
“…Gamma rays can cause displacement damage in materials through high-energy electrons and positrons that are produced through gamma-material interactions, Compton scattering, pair production and the photoelectric effect [35]. It was confirmed that electron irradiation with energies of several MeV causes hardening in low-alloy steels [36][37][38]. For thermal neutron effects, the contributions to displacement damage production and additional damage production through the nuclear reaction of boron were discussed.…”
Section: Influences Of Irradiation Variablesmentioning
confidence: 94%
“…The formation of Cu-rich clusters was detected at fluences of the order of 10 17 n/cm 2 by using the PA-CDB technique. Figure 6 shows an example of CDB spectra in 0.12%Cu A533B steel irradiated in a MTR at 290 • C, showing the rise of the Cu peak at 1 mdpa (∼5 × 10 17 n/cm 2 ) [37]. The coarsening of Cu-rich clusters (increase in size and decrease in density) is known to occur in high-Cu model alloys, and was also recently reported in surveillance specimens (0.3%Cu) at high fluences [53].…”
Section: Characteristics Of Solute Clustersmentioning
Current phenomenological knowledge and understanding of mechanisms are reviewed for radiation embrittlement of reactor pressure vessel low alloy steels and irradiation assisted stress corrosion cracking of core internals of stainless steels. Accumulated test data of irradiated materials in light water reactors and microscopic analyses by using state-of-the-art techniques such as a three-dimensional atom probe and electron backscatter diffraction have significantly increased knowledge about microstructural features. Characteristics of solute clusters and deformation microstructures and their contributions to macroscopic material property changes have been clarified to a large extent, which provide keys to understand in the degradation mechanisms. However, there are still fundamental research issues that merit study for long-term operation of reactors that requires reliable quantitative prediction of radiation-induced degradation of component materials in low-dose rate high-dose conditions.
“…The root of the volume fraction determined by 3DAP analysis is proportional to the transition temperature shift and the increase in hardness or yield strength. This relationship is widely found in surveillance data [59,69,71], MTR irradiation data [77,79] and also various changed particle irradiation data [37], and is irrespective of the Cu content and irradiation conditions. Figure 8 shows an example of the linear relationship between the cluster volume fraction and transition temperature shift [59].…”
Section: Characteristics Of Solute Clusterssupporting
confidence: 53%
“…Gamma rays can cause displacement damage in materials through high-energy electrons and positrons that are produced through gamma-material interactions, Compton scattering, pair production and the photoelectric effect [35]. It was confirmed that electron irradiation with energies of several MeV causes hardening in low-alloy steels [36][37][38]. For thermal neutron effects, the contributions to displacement damage production and additional damage production through the nuclear reaction of boron were discussed.…”
Section: Influences Of Irradiation Variablesmentioning
confidence: 94%
“…The formation of Cu-rich clusters was detected at fluences of the order of 10 17 n/cm 2 by using the PA-CDB technique. Figure 6 shows an example of CDB spectra in 0.12%Cu A533B steel irradiated in a MTR at 290 • C, showing the rise of the Cu peak at 1 mdpa (∼5 × 10 17 n/cm 2 ) [37]. The coarsening of Cu-rich clusters (increase in size and decrease in density) is known to occur in high-Cu model alloys, and was also recently reported in surveillance specimens (0.3%Cu) at high fluences [53].…”
Section: Characteristics Of Solute Clustersmentioning
Current phenomenological knowledge and understanding of mechanisms are reviewed for radiation embrittlement of reactor pressure vessel low alloy steels and irradiation assisted stress corrosion cracking of core internals of stainless steels. Accumulated test data of irradiated materials in light water reactors and microscopic analyses by using state-of-the-art techniques such as a three-dimensional atom probe and electron backscatter diffraction have significantly increased knowledge about microstructural features. Characteristics of solute clusters and deformation microstructures and their contributions to macroscopic material property changes have been clarified to a large extent, which provide keys to understand in the degradation mechanisms. However, there are still fundamental research issues that merit study for long-term operation of reactors that requires reliable quantitative prediction of radiation-induced degradation of component materials in low-dose rate high-dose conditions.
“…The yield strength at 290°C is 570 MPa. In the previous studies, it was confirmed that well-defined solute clusters and dislocation loops form in this material under neutron, electron, and heavy-ion irradiations in unstressed condition [15][16][17][18][19].…”
Section: Specimen Preparation and Irradiation Conditionssupporting
confidence: 52%
“…Although Ga atoms which were used in FIB micro-processing were also detected in these specimens of the elemental maps, the implanted Ga concentration was estimated as 0.1 at%, which was a negligibly low level. In order to obtain quantitative data on the cluster formation, elemental maps were analyzed based on the clustering of Si and Cu atoms which were recognized as the main elements constituting the core of solute clusters in the previous studies [15][16][17][18][19]. The clustering of Si atoms was most clearly observed in both specimens, and the clustering of Mn and Ni atoms was identified in the same position as the Si clustering.…”
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