Growth-rates of Single Crystals of Ethylene Diamine d-Tartrate: Flawed Growth and its Inhibition by Boric Acid

Booth, A. H.; Buckley, Harold E.

doi:10.1038/169367a0

Cited by 19 publications

(6 citation statements)

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“…Besides Beck's study, similar instabilities in the crystal growth rates have been observed by Booth and Buckley (1952) for ethylenediamine d-tartrate, and by Mullin and Garside (1967a) for the (100) faces of potassium alum.…”

Section: Methodssupporting

confidence: 73%

Growth Rates of Aluminum Potassium Sulfate Crystals in Aqueous Solutions

Botsaris¹,

Denk²

1970

Ind. Eng. Chem. Fund.

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Section: Methodssupporting

confidence: 73%

Growth Rates of Aluminum Potassium Sulfate Crystals in Aqueous Solutions

Botsaris¹,

Denk²

1970

Ind. Eng. Chem. Fund.

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“…Though the crossover between G−σ isotherms can be caused by mechanism competition, hence resulting in a disordered growth rate dependence on temperature, the growth decrease with the increase of temperature at the first stage may also be caused by impurities which could be induced during the crystal mounting process. Impurity caused growth rates divergence can be found in the literature. − But to confirm this hypothesis, further experiments need to be conducted.…”

Section: Resultsmentioning

confidence: 96%

“…Impurity caused growth rates divergence can be found in literature. [52][53][54][55] But to confirm this hypothesis, further experiment needs to be conducted.…”

Section: Comparison With Growth Rate Data From Literaturementioning

confidence: 99%

Measurement of Crystal Face Specific Growth Kinetics

Cai

Liu

et al. 2016

Crystal Growth & Design

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An instrument for measurement of face specific growth kinetics of crystals growing in a solution is developed and applied to crystallization of sodium nitrate (NaNO3) and potassium dihydrogen phosphate (KH2PO4, KDP). The device consists of three major components, a stereovision imaging system that captures in real-time the size change in each face direction of the crystal, an ATR-FTIR probe measuring solution concentration and supersaturation, and a small purpose-designed crystallizer that allows a crystal to be fixed in the solution and adequate solution mixing so the concentration measured can reflect the solution concentration near the surfaces of the crystal. The growth rates of all independent faces of NaNO3 and KDP crystals were derived at each time interval. For the NaNO3 crystal, growth rates in the temperature range of 298.15 ~ 318.15 K and supersaturation range of 0.01 ~ 0.11 were measured, enabling a systematic kinetic study. For the KDP crystal, the growth rates were measured just to show the capability of the system in handling crystals with different morphologies.

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“…[13][14][15][16]). For our experiments that are presented here, a crystal that had been commercially grown by JENA-CRYSTAL GbR, Jena, was used.…”

Section: Crystallographic Aspects Of Edtmentioning

confidence: 97%

“…In the course of investigations in the Bell Telephone Laboratories to find a substitute for quartz for expanding telephone needs in the late 1940s, crystal growth of ethylenediamine (+)-tartrate was raised to commercial level and in the following some physical properties of the crystals were determined (see Table 2 and e.g. [13][14][15][16]). For our experiments that are presented here, a crystal that had been commercially grown by JENA-CRYSTAL GbR, Jena, was used.…”

Section: Crystallographic Aspects Of Edtmentioning

confidence: 99%