Gas Chromatography of Solid Organic Compounds

Flame Response in the Quantitative Determination of High Molecular Weight Paraffins and Alcohols by Gas Chromatography.

“…The amount of reaction is measured after a specified time, and is related to the original concentration by reference to a calibration curve prepared from the analysis of known mixtures under the same conditions. A procedure for the determination of internal and external double bonds in polymers also uses the rates of reaction with perbenzoic acid (8).…”

Low Temperature Gas Chromatography

“…The number of theoretical plates for systems of n-heptane on brick was about 100 per foot. Such low values are apparently enhanced (see Figure 1) by other factors such as reduced temperature in achieving separation of similar components ( , 6).…”

Observations on the Effects of Temperature, Support, and Amount of Partitioning Liquid in Gas Chromatography.

“…and HIS COWORKERS (4,5) were the first to suggest that small weight-percentages of partitioning liquid on glass microbeads and small samples be combined to lower the column temperature and thereby decrease the chance of decomposing high-boiling substances. Glass beads were selected because their low specific surface area would decrease the amount of tailing due to adsorption by the support at the low7 liquid loadings employed.…”