Gas chromatography in inorganic chemistry

Tadmor, J.

doi:10.1016/0009-5907(63)81014-5

Cited by 12 publications

(2 citation statements)

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“…The GC apparatus consisted of a glass column and furnace, described elsewhere (21). The stationary phase consisted of Sil-O-Cel insulating fire brick (Johns-Manville) and Alundum (Norton Co.) of different mesh sizes, either uncoated or coated with a liquid layer.…”

Section: The Separation Potentialitiesmentioning

confidence: 99%

“…The sample of metal chloride was injected into the column and the isotopic exchange between the chlorine of the metal chlorides and the Cl36 retained on the stationary phase, as well as concentration profiles, were determined by counting the activity of the eluted material with a 20th Century Electronic liquid beta counter (type M6) connected to an Atomic Scaler, Model 1091. Counting of the activity of the effluent with a liquid counter was made possible by washout of the gaseous effluent with a solvent stream (21).…”

Section: The Separation Potentialitiesmentioning

confidence: 99%

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Applications of Isotopic Exchange in Gas Chromatography.

Tadmor¹

1964

Anal. Chem.

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disulfide was examined for purity chroma to graphically and was observed to be 95 to 99% pure. At the same time, it was evident that peak 20 was not being produced in the instrument from the disulfide because none was present in these purity runs. It is suspected that the diallyl disulfide disproportionates to a small extent upon standing, since both the trisulfide and monosulfide were observed in approximately equimolar quantities in the standard.The purified diallyl disulfide was used for the previously mentioned trisulfide synthesis, and the main peak observed after this reaction compared with peak 20 in both retention time and value.

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Section: The Separation Potentialitiesmentioning

confidence: 99%

Section: The Separation Potentialitiesmentioning

confidence: 99%