2010
DOI: 10.1557/jmr.2010.0083
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Formation of metal microspheres by ultrasonic cavitation

Abstract: A new physical method is described for the preparation of metal microspheres by ultrasonic cavitation of low-melting point metals (<380 °C) immersed in hot silicone oil. The ultrasonic radiation causes dispersion of the molten metals into spheres, which solidify rapidly on cooling. This method is illustrated for the synthesis of Pb and Au–Si eutectic alloy.

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Cited by 20 publications
(10 citation statements)
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“…14 We have recently reported on the formation of gallium microspheres by ultrasonic irradiation of molten gallium in either water or in silicone oil. [15][16][17] The microspheres are formed via the cavitation process which occurs in the liquid and involves the formation, growth and energetic collapse of gas bubbles. The collapse of the acoustic bubble causes dispersion of the molten gallium into nanometric to micrometric spheres which remain stable and do not coalesce aer irradiation is ceased, even though the temperature of the suspension is higher than the melting point of gallium (29.8 C).…”
Section: Introductionmentioning
confidence: 99%
“…14 We have recently reported on the formation of gallium microspheres by ultrasonic irradiation of molten gallium in either water or in silicone oil. [15][16][17] The microspheres are formed via the cavitation process which occurs in the liquid and involves the formation, growth and energetic collapse of gas bubbles. The collapse of the acoustic bubble causes dispersion of the molten gallium into nanometric to micrometric spheres which remain stable and do not coalesce aer irradiation is ceased, even though the temperature of the suspension is higher than the melting point of gallium (29.8 C).…”
Section: Introductionmentioning
confidence: 99%
“…Metal droplets can be fabricated by ultrasonic cavitation when low-melting-point metals mix with hot silicone [84,85]. Similarly, ultrasonic cavitation is also suitable for fabrication of LM micro/nanodroplets [86][87][88][89].…”
Section: Fabrication Of Pure Liquid Metal Dropletsmentioning
confidence: 99%
“…The Pb microparticles are made in-house using ultrasonic cavitation [41], which yields near-spherical particles with a distribution of diameters between 0.5 µm and 200 µm. The tin-lead microspheres of 50 µm diameter are commercially available (Easy-Spheres).…”
Section: Superconducting Microparticlesmentioning
confidence: 99%