2012
DOI: 10.2478/v10063-012-0004-7
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Fly-ash:H2O Assisted Aldol Condensation: Effect of Solvents on the Synthesis of Some Aryl (E) 2-propen-1-ones

Abstract: Some series of aryl (E) 2-propen-1-ones have been synthesized by Fly-ash:H20 catalyzed aldol condensation of aryl methyl ketones and substituted benzaldehydes at reflux condition in atmospheric pressure. The yields of chalcones are higher than 60%. These chalcones were characterized by their physical constants and spectral data, for known compounds their purities were checked with the physical constants and spectral data earlier published in the literature. The effects of solvents on the product have been stud… Show more

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Cited by 3 publications
(3 citation statements)
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“…An equi-molar quantities of 1-acetylpyrene (2 mmol) and substituted benzaldehydes (2 mmol), Fly-ash(0.5 g) with 20 mL of water [19,31] (Scheme 1) were refluxed for 4h. and the completion of the reaction was monitored by thin layer chromatography.…”
Section: Synthesis Of Chalconesmentioning
confidence: 99%
“…An equi-molar quantities of 1-acetylpyrene (2 mmol) and substituted benzaldehydes (2 mmol), Fly-ash(0.5 g) with 20 mL of water [19,31] (Scheme 1) were refluxed for 4h. and the completion of the reaction was monitored by thin layer chromatography.…”
Section: Synthesis Of Chalconesmentioning
confidence: 99%
“…All substituted 2,4-dimethoxy phenyl chalcones were synthesized by procedure published in literature [19,31]. An equi-molar quantities of 2,4-dimethoxy acetophenone (2 mmol) substituted benzaldehydes (2 mmol), Fly-ash (0.5 g) and 20 mL of water (Scheme 1) were refluxed for 4h.…”
Section: Synthesis Of Chalconesmentioning
confidence: 99%
“…All substituted styryl-1-pyrenyl chalcones were synthesized by procedure published in literature. An equi-molar quantities of 1-acetylpyrene (2 mmol) and substituted benzaldehydes (2 mmol), Fly-ash(0.5 g) with 20 mL of water [19,31] (Scheme 1) were refluxed for 4h. and the completion of the reaction was monitored by thin layer chromatography.…”
Section: Synthesis Of Chalconesmentioning
confidence: 99%