Facile synthesis of nickel@carbon nanorod composite for simultaneously electrochemical detection of dopamine and uric acid

Liu, Bo-Tao; Cai, Xin-Qin; Luo, Yu‐Hui; Zhu, Kenny Q.; Zhang, Qingyu; Hu, Tong-Tong; Sang, Tingting; Zhang, Chengyan; Zhang, Dongen

doi:10.1016/j.microc.2021.106823

Cited by 15 publications

(7 citation statements)

References 45 publications

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Section: Resultssupporting

confidence: 85%

“…The sensitivity, limit of detection (LOD) based on 3 S b /m, and limit of quantification (LOQ) based on 10 S b /m (S b is the standard deviation of the blank signals for n = 3, and m is the slope of the calibration plot) are estimated as 2.033 µA µM −1 cm −2 , 0.016 µM, and 0.053 mM, respectively. The proposed Ni-Co-P NSs/Nafion/GCE showed good comparability with some previous reports concerning electrochemical non-enzymatic DA sensors based on different transition-metal (including metal Ni, Co, or Ni/Co) compound materials (Table 1) [39,[43][44][45][46][47]. rate = 20 mVs −1 , modulation time = 0.05 s, internal time = 0.2 s, and step potential = 0.004 V. Figure 8a shows the DPV response at Ni-Co-P NSs/Nafion/GCE with increasing DA concentrations from 0 to 50 It is evident that the DPV response increased with the increase in DA concentration, and the inset of Figure 8a shows an amplified view of the DPV responses in the low-concentration region.…”

Section: Resultssupporting

confidence: 84%

“…Ag-ZIF-67p/GCE 0.10~100 1.469 0.050 [39] Ni@CNRs/GCE 0.50~30 0.379 0.056 [43] Ni-BTC@Ni 3 S 4 /CPE 0.05~750 0.560 0.016 [44] Ni-MOF/GCE 0.20~100 0.285 0.060 [45] NiO/NiCo 2 O 4 /CPE 0.10~100 -0.040 [46] Ni 2 Co-LDH/GCE 1.30~420 0.148 1.250 [47] Ni-Co-P NSs/Nafion/GCE 0.3~50 2.033 0.016 This Work…”

Section: Detection Limit (µM) Referencementioning

confidence: 99%

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Enhancing Electrochemical Non-Enzymatic Dopamine Sensing Based on Bimetallic Nickel/Cobalt Phosphide Nanosheets

Wang,

Tsai,

Chang

et al. 2024

Micromachines

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In this study, the successful synthesis of bimetallic nickel/cobalt phosphide nanosheets (Ni-Co-P NSs) via the hydrothermal method and the subsequent high-temperature phosphorization process were both confirmed. Ni-Co-P NSs exhibited excellent electrocatalytic activity for the electrochemical non-enzymatic DA sensing. The surface morphologies and physicochemical properties of Ni-Co-P NSs were characterized by atomic force microscopy (AFM), field-emission scanning (FESEM), field-emission transmission electron microscopy (FETEM), and X-ray diffraction (XRD). Further, the electrochemical performance was evaluated by cyclic voltammetry (CV) and differential pulse voltammetry (DPV). The metallic nature of phosphide and the synergistic effect of Ni/Co atoms in Ni-Co-P NSs provided abundant catalytic active sites for the electrochemical redox reaction of DA, which exhibited a remarkable consequence with a wide linear range from 0.3~50 μM, a high sensitivity of 2.033 µA µM−1 cm−2, a low limit of detection of 0.016 µM, and anti-interference ability. As a result, the proposed Ni-Co-P NSs can be considered an ideal electrode material for the electrochemical non-enzymatic DA sensing.

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Section: Resultssupporting

confidence: 85%

Section: Resultssupporting

confidence: 84%

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Enhancing Electrochemical Non-Enzymatic Dopamine Sensing Based on Bimetallic Nickel/Cobalt Phosphide Nanosheets

Wang,

Tsai,

Chang

et al. 2024

Micromachines

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“…According to the slope ( S ) of the regression equations and standard deviation (Sb) of the mean values of 10 DPVs of the blank solution, LODs were calculated to be 6.32, 0.45, and 0.81 μM for AA, DA, and UA, respectively, by using the 3Sb/S equation [ 55 ]. Compared with other electrodes modified with various TMD- and CNF-based materials, the Co/MoSe 2 /PPy@CNF-modified GCE exhibits good and comparable analytical performance for the simultaneous determination of AA, DA, and UA (Table 1 ).…”

Section: Resultsmentioning

confidence: 99%

Electrospun cobalt-doped 2D-MoSe2/polypyrrole hybrid-based carbon nanofibers as electrochemical sensing platforms

Celik Cogal,

Cogal,

Machata

et al. 2024

Microchim Acta

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A novel cobalt-doped two-dimensional molybdenum diselenide/polypyrrole hybrid-based carbon nanofiber (Co/MoSe2/PPy@CNF) was prepared using the hydrothermal method followed by electrospinning technique. The structural and morphological properties of the 2D-TMD@CNF-based hybrids were characterized through X-ray photoelectron spectroscopy (XPS), scanning electron microscopy (SEM), energy-dispersive spectrometry (EDS), and transmission electron microscopy (TEM). The Co-MoSe2/PPy@CNF exhibited large surface area, porous structure, and improved active sites due to the synergistic effect of the components. The electrochemical and electrocatalytic characteristics of the 2D-TMD@CNF-modified electrodes were also investigated using cyclic voltammetry (CV) and differential pulse voltammetry (DPV) techniques. The Co/MoSe2/PPy@CNF electrode was used as an electrochemical sensor for simultaneous detection of ascorbic acid (AA), dopamine (DA), and uric acid (UA) and showed enhanced catalytic activity and sensitivity. Using DPV measurements, the Co/MoSe2/PPy@CNF demonstrated wide linear ranges of 30–3212 μM for AA, 1.2–536 μM for DA, and 10–1071 μM for UA with low detection limits of 6.32, 0.45, and 0.81 μM, respectively. The developed sensor with the Co/MoSe2/PPy@CNF-modified electrode was also applied to a human urine sample and gave recoveries ranging from 94.0 to 105.5% (n = 3) for AA, DA, and UA. Furthermore, the Co/MoSe2/PPy@CNF-based sensor exhibited good selectivity and reproducibility for the detection of AA, DA, and UA. Graphical abstract

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“…In terms of non-enzymatic-based assays, fluorescence spectrometry, liquid chromatography, and electroanalytical techniques are the most common non-enzymatic methods. 7,8 Among these, electrochemical recognition is considered a highly promising method due to its rapid response, high selectivity, low detection limit, and cost-effectiveness. The electrochemical method is considered a promising approach for UA detection.…”

Section: Introductionmentioning

confidence: 99%

Hierarchical sulfur-doped scaly carbon coupled with a cerium oxide nanoparticle-based electrochemical sensor for the sensitive determination of uric acid

Zhu,

Li,

et al. 2023

New J. Chem.

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Facile synthesis of nickel@carbon nanorod composite for simultaneously electrochemical detection of dopamine and uric acid

Cited by 15 publications

References 45 publications

Enhancing Electrochemical Non-Enzymatic Dopamine Sensing Based on Bimetallic Nickel/Cobalt Phosphide Nanosheets

Enhancing Electrochemical Non-Enzymatic Dopamine Sensing Based on Bimetallic Nickel/Cobalt Phosphide Nanosheets

Electrospun cobalt-doped 2D-MoSe2/polypyrrole hybrid-based carbon nanofibers as electrochemical sensing platforms

Hierarchical sulfur-doped scaly carbon coupled with a cerium oxide nanoparticle-based electrochemical sensor for the sensitive determination of uric acid

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