Facile sonochemical synthesis of porous and hierarchical manganese(III) oxide tiny nanostructures for super sensitive electrocatalytic detection of antibiotic (chloramphenicol) in fresh milk

Rajaji, Umamaheswari; Akilarasan, Muthumariappan; Chen, Shen‐Ming; Tseng, Tien‐Wen; Wang, Kang; Qi, Dongdong; Jiang, Jianzhuang

doi:10.1016/j.ultsonch.2019.104648

Cited by 32 publications

(22 citation statements)

References 49 publications

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“…The XRD patterns of the as synthesized NiCo 2 S 4 -Ms and NiCo 2 O 4 -MFs are shown in Figure 3A. The XRD pattern of NiCo 2 S 4 -Ms Figure 3Aa shows the characteristic peaks at 16…”

Section: Xrd and Xps Analysis Of Nico 2 S 4 -Ms And Nico 2 O 4 -Mfsmentioning

confidence: 99%

“…The synthesis method for NiCo2S4 and NiCo2O4 with various structures such as, micro flowers, nanoprism [11], nanoplates [12] and nanorods [13] and their electrocatalytic properties were previously reported. However, the hydrothermal method are more convenient to synthesis nanomaterials with different morphology then other available methods [14][15][16]. The chemical reaction in hydrothermal process occurs due to the influential high-temperature and pressure, which results the formation of exceptional products [17].…”

Section: Introductionmentioning

confidence: 99%

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An Ultra-Sensitive Electrochemical Sensor for the Detection of Carcinogen Oxidative Stress 4-Nitroquinoline N-Oxide in Biologic Matrices Based on Hierarchical Spinel Structured NiCo2O4 and NiCo2S4; A Comparative Study

Chen

Tamilalagan

Akilarasan

et al. 2020

IJMS

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Various factors leads to cancer; among them oxidative damage is believed to play an important role. Moreover, it is important to identify a method to detect the oxidative damage. Recently, electrochemical sensors have been considered as the one of the most important techniques to detect DNA damage, owing to its rapid detection. However, electrode materials play an important role in the properties of electrochemical sensor. Currently, researchers have aimed to develop novel electrode materials for low-level detection of biomarkers. Herein, we report the facile hydrothermal synthesis of NiCo2O4 micro flowers (MFs) and NiCo2S4 micro spheres (Ms) and evaluate their electrochemical properties for the detection of carcinogen-causing biomarker 4-nitroquinoline n-oxide (4-NQO) in human blood serum and saliva samples. Moreover, as-prepared composites were fabricated on a glass carbon electrode (GCE), and its electrochemical activities for the determination of 4-NQO were investigated by using various electrochemical techniques. Fascinatingly, the NiCo2S4-Ms showed a very low detection limit of 2.29 nM and a wider range of 0.005 to 596.64 µM for detecting 4-NQO. Finally, the practical applicability of NiCo2S4-Ms in the 4-NQO spiked human blood serum and saliva samples were also investigated.

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“…The XRD patterns of the as synthesized NiCo 2 S 4 -Ms and NiCo 2 O 4 -MFs are shown in Figure 3A. The XRD pattern of NiCo 2 S 4 -Ms Figure 3Aa shows the characteristic peaks at 16…”

Section: Xrd and Xps Analysis Of Nico 2 S 4 -Ms And Nico 2 O 4 -Mfsmentioning

confidence: 99%

Section: Introductionmentioning

confidence: 99%

An Ultra-Sensitive Electrochemical Sensor for the Detection of Carcinogen Oxidative Stress 4-Nitroquinoline N-Oxide in Biologic Matrices Based on Hierarchical Spinel Structured NiCo2O4 and NiCo2S4; A Comparative Study

Chen

Tamilalagan

Akilarasan

et al. 2020

IJMS

Self Cite

View full text Add to dashboard Cite

show abstract

“…Scientific investigations have revealed its effectivity in treating life-threatening diseases such as typhoid fever and childhood meningitis and septicaemia. However, the use of CPL has been restricted owing to its toxicity and excessive usage which causes gray-baby syndrome, aplastic anemia, and bone-marrow suppression [19] , [21] . Although certain restrictions were imposed in the usage of CPL by some nations, its out-and-out eradication is difficult by virtue of its application in wide range of production process, low-cost, and high availability [22] , [23] .…”

Section: Introductionmentioning

confidence: 99%

Effects of sonochemical approach and induced contraction of core–shell bismuth sulfide/graphitic carbon nitride as an efficient electrode materials for electrocatalytic detection of antibiotic drug in foodstuffs

Govindasamy

Wang

Almahri

et al. 2021

Ultrasonics Sonochemistry

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“…Nickel nanoparticles are widely used due to their unique properties, which include a large surface area to volume ratio, a low melting point, a low burning point, and high surface energy (Zhang, 2003). Ni NPs have applications in several fields like magnetic materials, aviation, ceramics, catalysts, and the biomedical field (Alam et al, 2018; Gao et al, 2017; Rajaji et al, 2019). The primary source of Ni NPs is inhalation while the data representing nickel NPs’ (Ni NPs) toxic effects are scarce (Ahamed, 2011).…”

Section: Introductionmentioning

confidence: 99%

Nickel nanoparticles induce hepatotoxicity via oxidative and nitrative stress-mediated apoptosis and inflammation

et al. 2021

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Nickel nanoparticles (Ni NPs) are utilized extensively in various industrial applications. However, there are increasing concerns about potential exposure to Ni NPs and consequent health effects. The aim of this study was to assess Ni NPs-induced liver toxicity in Sprague Dawley rats. Twenty-five rats were exposed to Ni NPs via intraperitoneal injection at doses of 15, 30, and 45 mg/kg per body weight for 28 days. Results from ICP-MS analysis showed an increase in the concentration of Ni NPs in a dose-dependent manner. The liver dysfunction was indicated by considerable production of ALT, AST, ALP, LDH, and TB in Ni NPs-treated rats. Histological examination demonstrated liver injuries (inflammatory cells, congestion, necrosis, and pyknosis) in exposed rats with dose-dependent severity of pathologies by semi-quantitative histograding system. To explore the toxicological pathways, we examined oxidative stress biomarkers and detected Ni NPs significantly elevated the levels of MDA and LPO while decreasing the levels of CAT and GSH. All the changes in biomarkers were recorded in a dose-dependent relationship. In addition, we found upregulated NF-kβ indicating activation of inflammatory cytokines. ELISA results of serum revealed a remarkable increase of nitrative stress markers (iNOS and NO), ATPase activity, inflammatory cytokine (IL-6, IL-1β, and TNF-α), and apoptotic mediators (caspase-3 and caspase-9) in Ni NPs-treated groups than the control. In summary, the result of this study provided evidence of hepatotoxicity of Ni NPs and insightful information about the involved toxic pathways, which will help in health risk assessment and management, related preventive measures for the use of Ni-NPs materials.

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Facile sonochemical synthesis of porous and hierarchical manganese(III) oxide tiny nanostructures for super sensitive electrocatalytic detection of antibiotic (chloramphenicol) in fresh milk

Cited by 32 publications

References 49 publications

An Ultra-Sensitive Electrochemical Sensor for the Detection of Carcinogen Oxidative Stress 4-Nitroquinoline N-Oxide in Biologic Matrices Based on Hierarchical Spinel Structured NiCo2O4 and NiCo2S4; A Comparative Study

An Ultra-Sensitive Electrochemical Sensor for the Detection of Carcinogen Oxidative Stress 4-Nitroquinoline N-Oxide in Biologic Matrices Based on Hierarchical Spinel Structured NiCo2O4 and NiCo2S4; A Comparative Study

Effects of sonochemical approach and induced contraction of core–shell bismuth sulfide/graphitic carbon nitride as an efficient electrode materials for electrocatalytic detection of antibiotic drug in foodstuffs

Nickel nanoparticles induce hepatotoxicity via oxidative and nitrative stress-mediated apoptosis and inflammation

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