2011
DOI: 10.1016/j.jallcom.2010.10.107
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Facile route to silver submicron-sized particles and their catalytic activity towards 4-nitrophenol reduction

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Cited by 44 publications
(17 citation statements)
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“…Generally, the Ag nanoparticles of sizes less than 20 nm are precipitated from Ag salts to form agglomerates with sizes ranging from 800 to 3500 nm [31]. Reducing agents like ascorbic acid [40,56], hydrazine monohydrate [57], sodium citrate [58] or sodium citrate dihydrate [59], polyvinylpyrollidone [50], ethylenediaminetetraacetic acid (EDTA) [60], sodium sulfite [61] and sodium borohydride [62] were added into Ag salts like nitrates, sulphates or chlorates or Ag-ammonia complexes [62]. The reducing reaction occurred in a polar solvent such as ethanol, methanol, acetonitrile or tetrahydrofurane [40].…”
Section: Synthesis Of Ag Nanoparticlesmentioning
confidence: 99%
“…Generally, the Ag nanoparticles of sizes less than 20 nm are precipitated from Ag salts to form agglomerates with sizes ranging from 800 to 3500 nm [31]. Reducing agents like ascorbic acid [40,56], hydrazine monohydrate [57], sodium citrate [58] or sodium citrate dihydrate [59], polyvinylpyrollidone [50], ethylenediaminetetraacetic acid (EDTA) [60], sodium sulfite [61] and sodium borohydride [62] were added into Ag salts like nitrates, sulphates or chlorates or Ag-ammonia complexes [62]. The reducing reaction occurred in a polar solvent such as ethanol, methanol, acetonitrile or tetrahydrofurane [40].…”
Section: Synthesis Of Ag Nanoparticlesmentioning
confidence: 99%
“…The catalytic reactivity of core-shell and pure metal oxide nanoparticles was studied by the reduction of 4-nitrophenol with NaBH 4 . This reaction has been used to test the reactivity of metal oxide nanoparticles [68,69]. An aqueous solution of 4-nitrophenol is yellow colored which on reduction with NaBH 4 become colorless due to the reduction of 4-nitrophenolate ions (yellow) to 4-aminophenolate ions (colorless) [70].…”
Section: Reaction Conditionmentioning
confidence: 99%
“…Chemical reduction method is the simplest process, widely used to obtain uniform, small size and highly disperse nanoparticles [24]. But chemical reduction method for the syntheses of nanoparticles has a big disadvantage of using toxic chemicals and formation of toxic byproducts, making nanoparticles unsuitable for biological purposes [25][26][27].…”
Section: Introductionmentioning
confidence: 99%