Extractive‐Spectrophotometric Determination of Beryllium as an Ion‐Association Complex with Alizarine Fluorine Blue and Adogen

Abstract

In t h i r paper, w e report a r e n r i t i v e method f o r determination of beryllium bared on formation of the Be(I1)-alizarine fluorine blue complex snd it. rubrequent extraction i n t o toluene with adogen. EXPERIMENTAL Reagent. AliZAtine fluorine blue : a H squewr rolution. Beryllium solution : a 1.000 g/l rolution of BeS04.4H20 i n 0.2 H hydrochloric acid. Mogen rolution : I g/l i n t o l u e w . Buffer : a 1.0 H T r i r / H C l buffar of pH 7.2 war prepared, A l l rolventr and reagentr ware of analytical grade.Apparatur 501 with calomel combinated electrode were ured. ProcadureA mixture containing lor. than 18 yg of beryllium, 10 ml of pH 7.2 buffer rolution and 10 m1 of